Teledyne 4060 - Manuals

Series 4060 Teledyne Analytical Instruments v Additional Safety Information DANGER COMBUSTIBLE GAS USAGE WARNING This is a general purpose instrument designed for use in a non-hazardous area. It is the customer's responsibility to ensure safety especially when combustible gases are being analyzed si...

Series 4060 Teledyne Analytical Instruments vii 3. External hazardous voltages which may be connected to the Analyzer alarm relay connections. Procedure for Removal of Internal Inaccessible Shock Hazards CAUTION: SERVICING OR MAINTENANCE OF THE ANALYZER SHOULD ONLY BE DONE BY SUITABLE TRAINED PERSON...

Series 4060 viii Teledyne Analytical Instruments WARNING: THIS INSTRUMENT IS DESIGNED TO BE OPERATED IN A NONHAZARDOUS AREA. THE ANALYZER USES HYDROGEN GAS AND/OR OTHER COMBUSTIBLE GASES IN ITS OPERATION. THIS EQUIPMENT, IF NOT USED AND MAINTAINED PROPERLY CAN BE AN EXPLOSION HAZARD. THE ANALYZER, D...

Series 4060 Teledyne Analytical Instruments ix Table of Contents Safety Messages .......................................................................... iii Additional Safety Information ...................................................... v List of Figures ........................................

Series 4060 x Teledyne Analytical Instruments 3.3 User Connections 28 3.3.1 Electrical Power Connections 28 3.3.2 Electronic Connections 28 3.3.2.1 Primary Input Power 29 3.3.2.2 Fuse Installation 30 3.3.2.3 50-Pin Equipment Interface Connector 30 3.3.2.4 Analog Output 30 3.3.2.5 Alarm Relays 32 3.3...

Series 4060 Teledyne Analytical Instruments xi 4.5 Sample Pump 44 4.6 Analyzer Operation 44 4.6.1 Default Parameters 46 4.6.2 Style Conventions 46 4.6.3 Navigation and Data Entry 47 4.6.3.1 Arrow Keys 47 4.6.3.2 ENTER 47 4.6.3.3 ESCAPE 48 4.6.4 Menu Structure 48 4.6.4.1 Main Menus 49 4.6.5 Span 50 4...

Series 4060 xii Teledyne Analytical Instruments 5.1.4 Collector Cable 68 5.2 Temperature Control Electronic Check 68 5.3 Ignition and/or Flame Guard Circuit Checks 69 5.4 Sampling System 70 5.5 Printed Circuit Board Descriptions 71 5.5.1 Flame Guard and Anode Power Supply PCB 71 5.5.2 Proportional T...

Series 4060 Teledyne Analytical Instruments xiii List of Figures Figure 1-1: Model 4060 Front Panel Interface ............................... 17   Figure 1-2: Model 4060 Rear Panel .............................................. 17   Figure 2-1: Internal Temperature Controllers .........................

Series 4060 xiv Teledyne Analytical Instruments List of Tables Table 3-1: Analog Output Connections ......................................... 31 Table 3-2: Analog Concentration Output—Example ..................... 31 Table 3-3: Analog Range ID Output—Example ............................. 32 Table 3-...

Series 4060 Introduction Teledyne Analytical Instruments 15 Introduction Teledyne Analytical Instruments Series 4060, Trace Aromatic Hydrocarbon Analyzer, is a versatile instrument designed to measure the quantity of aromatic hydrocarbons, primarily benzene, present in a positive pressure sample gas...

Introduction Series 4060 16 Teledyne Analytical Instruments  Extensive self-diagnostic testing at startup and on demand with continuous power supply monitoring.  RS-232 serial digital port for use with a computer or other digital communication device.  Analog outputs for concentration and range i...

Series 4060 Introduction Teledyne Analytical Instruments 17 Figure 1-1: Model 4060 Front Panel Interface Figure 1-2: Model 4060 Rear Panel

Introduction Series 4060 18 Teledyne Analytical Instruments 1.4 Applications  Monitoring the benzene concentration of carbon dioxide gas for use in the beverage industry.  Monitoring aromatic contamination in air liquefaction and other gas production processes.  Gas purity certification.  Detect...

Series 4060 Operational Theory Teledyne Analytical Instruments 19 Operational Theory 2.1 Introduction Series 4060 Analyzer for Benzene uses a FID detector and a Gas Chromatograph (GC) Column. Using a carrier gas and a microprocessor actuated switching valve, a fixed volume of sample is pushed into t...

Operational Theory Series 4060 20 Teledyne Analytical Instruments 1. Valve Position A— Sampling Mode In this mode the analyzer configures the operational valve to back flush the column and charge the sample loop. The Sample Mode is programmed to continue for a 7 minute period by factory default; how...

Series 4060 Operational Theory Teledyne Analytical Instruments 21 analyzer chassis. They are accessible by opening the front door of the analyzer . Adjustments are made using the appropriate control on the front panel. The analyzer contains three separate isothermal chambers ‘SAMPLE’, ‘FID’, and ‘CO...

Operational Theory Series 4060 22 Teledyne Analytical Instruments supplied at constant pressures using two stage stainless steel diaphragm gas regulators. The recommended pressure range is 30 to 8 0 psig, however, the span gas should be supplied at a pressure of 20 psig to the restrictor fitting eit...

Series 4060 Operational Theory Teledyne Analytical Instruments 23 Figure 2-2: Typical Piping Diagram for the Model 4060

Operational Theory Series 4060 24 Teledyne Analytical Instruments 2.4 Detection Cell The upper section of the stainless steel flame ionization cell houses the cylindrical collector electrode, the high voltage (+260 VDC) anode-igniter coil, and the sensing thermistor of the flame guard circuit (see c...

Series 4060 Operational Theory Teledyne Analytical Instruments 25 2.4.1 Electrometer-Amplifier The collector cable is coupled directly to a coaxial fitting located on the electrometer-amplifier PC board. The PC board is located on the side panel next to but outside of the isothermal chamber. It cons...

Operational Theory Series 4060 26 Teledyne Analytical Instruments 2.4.2 Anode Power Supply The high voltage anode power supply components are mounted on the anode power supply printed circuit board. High voltage regulation is achieved through the use of series-connected zener diodes. The simplicity ...

Series 4060 Installation Teledyne Analytical Instruments 27 Installation Installation of the Series 4060 Analyzer includes: 1. Unpacking 2. Mounting 3. Gas connections 4. Electrical connections 5. Testing the system. 3.1 Unpacking the Analyzer Although the analyzer is shipped with all the materials ...

Installation Series 4060 28 Teledyne Analytical Instruments levers found almost at the end of the sliders, both sides at the same time. Regardless of configuration, the analyzer/system must be installed on a level surface with sufficient space allocated on either side for personnel and test equipmen...

Series 4060 Installation Teledyne Analytical Instruments 29 For safe connections, no uninsulated wiring should be able to come in contact with fingers, tools or clothing during normal operation. CAUTION: USE SHIELDED CABLES. ALSO, USE PLUGS THAT PROVIDE EXCELLENT EMI/RFI PROTECTION. THE PLUG CASE MU...

Installation Series 4060 30 Teledyne Analytical Instruments 3.3.2.2 F USE I NSTALLATION The fuse block, at the right of the power cord receptacle, accepts US or European size fuses. A jumper replaces the fuse in whichever fuse receptacle is not used. 3.3.2.3 50-P IN E QUIPMENT I NTERFACE C ONNECTOR ...

Series 4060 Installation Teledyne Analytical Instruments 31 Table 3-1: Analog Output Connections Pin Function 3 Channel 2, + 4-20 mA, floating 4 Channel 2, – 4-20 mA, floating 5 Channel 1, + 4-20 mA, floating 6 Channel 1, – 4-20 mA, floating 8 Channel 2, 0-1 VDC 23 Channel 2, 0-1 VDC, negative groun...

Installation Series 4060 32 Teledyne Analytical Instruments 40 0.4 10.4 50 0.5 12.0 60 0.6 13.6 70 0.7 15.2 80 0.8 16.8 90 0.9 18.4 100 1.0 20.0 Table 3-3: Analog Range ID Output—Example Range Voltage Signal Current Signal Application Output (VDC) Output (mA DC) Range 1 0.20 7.2 0–100 ppb Benzene Ra...

Series 4060 Installation Teledyne Analytical Instruments 33 Threshold Alarm 2:  Can be configured as high (actuates when concentration is above threshold), or low (actuates when concentration is below threshold).  Can be configured as failsafe or non-failsafe  Can be configured as non-latching  ...

Installation Series 4060 34 Teledyne Analytical Instruments 3.3.2.6 D IGITAL R EMOTE C AL I NPUTS The digital remote calibration input accepts 0 V (off) or 24 VDC (on) for remote control of calibration. (See Remote Calibration Protocol below.) See Table 3-5 for pin connections. Span: Floating input....

Series 4060 Installation Teledyne Analytical Instruments 35 2. When the CRC closes, remove the span command. When CRC opens again, the span calibration is done, and the sample is being analyzed. 3.3.2.7 R ANGE ID R ELAYS There are three dedicated Range ID relay contacts. They are assigned to relays ...

Installation Series 4060 36 Teledyne Analytical Instruments Table 3-7: Pin out of 50 pin D-Sub Connector pin # Description pin # Description 1 26 2 27 3 + Output 4-20 ma - Channel 2 28 Alarm 1 C Contact 4 - Output 4-20 ma - Channel 2 29 5 + Output 4-20 ma – Channel 1 30 6 - Output 4-20 ma – Channel ...

Series 4060 Installation Teledyne Analytical Instruments 37 Table 3-8: Commands via RS-232 Input Command Description AS <enter> Immediately starts an autospan. AL <enter> Immediately revert to Analyze (CH4 Mode) RL <enter> Change to Manual Range LOW RM <enter> Change to Manua...

Installation Series 4060 38 Teledyne Analytical Instruments Figure 3-3: Gas Connections Gas connections to the instrument are made at the 1/8”or 1/4” stainless steel tube fittings provided on the rear panel. Note that the Purge and Sensor Vent fittings are 1/4” while all other gas connections are 1/...

Series 4060 Installation Teledyne Analytical Instruments 39 not representative of the current contents of the line, or which might keep contaminants from being purged out of the system. CAUTION: THE GASES USED MUST BE OF THE HIGHEST QUALITY, ULTRA ZERO GRADES, AS SHOWN BELOW. FAILURE TO DO SO WILL R...

Installation Series 4060 40 Teledyne Analytical Instruments Addenda included with this manual to determine if special conditions apply. 3.3.3.1 E FFLUENT All the gases introduced into the detection cell vent from one fitting at the rear of the analyzer. TAI recommends that the cell be permitted to v...

Series 4060 Operation Teledyne Analytical Instruments 41 Operation This section of the manual describes how to setup and operate the Model 4060 Analyzer. Sections 4.1 through 4.5 describe preliminary steps and equipment needed to operate the analyzer. Beginning with Section 4.6, the actual operation...

Operation Series 4060 42 Teledyne Analytical Instruments CAUTION: THE GASES USED MUST BE OF THE HIGHEST QUALITY, ULTRA ZERO GRADES, AS SHOWN BELOW. FAILURE TO DO SO WILL RESULT IN CONTAMINATION AND FAILURE TO DETECT LOW PPB BENZENE. AIR: USE WATER PUMPED AIR WITH THC LESS THAN 0.1 PPM. DO NOT USE OI...

Series 4060 Operation Teledyne Analytical Instruments 43 4.3.1 Air 1. Set the air source regulator to 40 psig. 2. Adjust the analyzer air regulator until the air pressure gauge reads the recommended air pressure of 7.0 psig. After the air is flowing through the sensor and warm-up time has been compl...

Operation Series 4060 44 Teledyne Analytical Instruments factory. If the ignition process fails, the instrument will attempt to ignite the flame 4 more times. If it continues to fail after the fifth attempt, a flame failure message will appear on the display. If this occurs refer to Section 5. 4.4.1...

Operation Series 4060 46 Teledyne Analytical Instruments 4.6.1 Default Parameters The versatility of this analyzer usually results in significant changes being made to parameters over the course of time to better suit a particular application. Occasionally processes change requiring alteration to al...

Series 4060 Operation Teledyne Analytical Instruments 47 particular key it will be typed as text using all caps. Example: this is the ENTER key. Screen Modes: Times New Roman 12 pt. italic. Example: Analysis Mode or Setup Mode. Screen Readout: Arial Narrow, 12 pt bold. Example: AUTOCAL. 4.6.3 Naviga...

Operation Series 4060 48 Teledyne Analytical Instruments 1. When the selected option is a function on the MAIN MENU or any SUB MENU screen, the function name appears with an arrow next to it . In some cases, the item in the menu is the parent of another SUB MENU , in other cases, the item in the men...

Series 4060 Operation Teledyne Analytical Instruments 49 2. The MAIN MENU and SUB MENU screens have a flashing arrow on the left side indicating which item is being pointed to. 3. MODIFIABLE ITEM screens have a flashing value somewhere in the line. 4.6.4.1 M AIN M ENUS The MAIN MENU consists of 15 f...

Operation Series 4060 50 Teledyne Analytical Instruments  GROUP SETUP : Determines compound names, associated timing and measurement ranges. Do not change these.  PSWD: Used to establish password protection or change the existing password.  LOGOUT: Logging out prevents unauthorized tampering with...

Series 4060 Operation Teledyne Analytical Instruments 51 ________________________________________________ Begin Span: ENTER-YES ESCAPE-NO ________________________________________________ Pressing <Enter> enters the SPAN mode in the Sampling Phase. This is similar to the Analysis Mode both in t...

Operation Series 4060 52 Teledyne Analytical Instruments To initiate a self-test: < UP/DOWN >From the MAIN MENU scroll to the SELF-TEST function. < Enter > Activate the SELF-TEST function by pressing <Enter>. This brings up the SELF-TEST initialization screen. _____________________...

Series 4060 Operation Teledyne Analytical Instruments 53 -> AL-1 DEFEATED AL-1 HIGH AL-1 NON-FAILSAFE AL-1 NON-LATCHING AL-1 20.00 ppb AL-2 ACTIVE AL-2 LOW AL-2 FAILSAFE AL-2 LATCHING AL-2 50.00 ppb ________________________________________________ Note: For the purpose of example, Alarm 2 has bee...

Operation Series 4060 54 Teledyne Analytical Instruments LATCHING: The latching property configures the alarm such that the user must manually relieve the alarm condition even though the concentration no longer violates the trip point of the alarm. So, if an alarm is NON-LATCHING, and the analysis c...

Operation Series 4060 56 Teledyne Analytical Instruments ______________________________________________ -> CH1 Offset CH1 Gain CH1 (Wave, Id for Ch2, or Group Output) CH1 (Select Groups) CH2 (Wave, Id for Ch2, or Group Output) CH2 (Select Groups) ______________________________________________ 4.6...

Series 4060 Operation Teledyne Analytical Instruments 57 the Span functions as described in Section 4.6.5, and follow the precautions given there. Auto Span performs a span calibration using the target span value set in the Span feature menu. Note: If you require highly accurate AUTOCAL timing, use ...

Operation Series 4060 58 Teledyne Analytical Instruments Note: For instruction on how to set the parameters, please refer to the Data Entry section. The first line tells how soon the next automatic span will occur. Pressing <Enter> on this line has no effect. The second line Enables/Disables t...

Series 4060 Operation Teledyne Analytical Instruments 59 If user has LOGGED OUT, then only the following SUB MENU procedures may be executed: 1. PASSWORD 2. LOGOUT (which only repeats the logout) 3. MODEL Note however, that the instrument can still be used for analysis without entering the password....

Operation Series 4060 60 Teledyne Analytical Instruments ENTER PASSWORD SCREEN ________________________________________________ Enter a Password 'T' 'A' 'I' ________________________________________________ < UP/DOWN >Use the UP/DOWN keys to change the letters to the proper password. < Enter...

Series 4060 Operation Teledyne Analytical Instruments 61 < UP/DOWN >Use the UP/DOWN keys to change the letters to the new password. < Enter > Press <Enter> to advance to the next letter < Enter > The last <Enter> moves to the REPEAT PASSWORD ENTRY screen. < Escape &g...

Series 4060 Operation Teledyne Analytical Instruments 63 < UP/DOWN >From the MAIN MENU, scroll to the STANDBY function using the UP/DOWN keys. < Enter > Pressing <Enter> places the instrument in STANDBY. To exit STANDBY, scroll again to the STANDBY function and press <Enter> ...

Series 4060 Maintenance Teledyne Analytical Instruments 65 Maintenance & Troubleshooting WARNING: DANGEROUS HIGH VOLTAGES EXIST INSIDE THIS INSTRUMENT. THERE ARE NO USER SERVICEABLE PARTS WITHIN THE COVER ON THE INSIDE OF THE DOOR, INSIDE THE ISOTHERMAL CHAMBER, (SAMPLE SYSTEM), AND ON THE ELECT...

Maintenance Series 4060 66 Teledyne Analytical Instruments attempt to evaluate performance on sample gas. If analyzer sensitivity is questionable, use the span gas. For all other evaluations, use the zero gas and low range for maximum sensitivity. The important consideration is to control as many va...

Series 4060 Maintenance Teledyne Analytical Instruments 67 2. If no reading is obtained, disconnect the anode-igniter cable and check for the voltage on pin “J4-1” of the connector located at PC board part number B74671. If the proper voltage is still not present, replace the flame guard and anode p...

Maintenance Series 4060 68 Teledyne Analytical Instruments Whenever the flame guard and anode power supply printed circuit board have been replaced the analyzer must be recalibrated. If the instrument performs as outlined in this section, the problem is not related to the measuring circuit electroni...

Series 4060 Maintenance Teledyne Analytical Instruments 69 measure resistance between that wire and the remaining undisturbed terminal. Resistance of the thermistor varies with its surrounding temperature. A reading of between 10KOhms and 16Kohms at around 25°C may be measured. (Under very cold cond...

Series 4060 Maintenance Teledyne Analytical Instruments 71 5.5 Printed Circuit Board Descriptions The electronics circuitry of the analyzer is designed with the latest integrated circuit technology. The individual circuits which are required to process the incoming signal and condition it to provide...

Maintenance Series 4060 72 Teledyne Analytical Instruments 5.5.2 Proportional Temperature Controller PCB Schematic No. B-30974 Assembly Dwg. No. B-30927 The temperature of the chamber to be controlled is regulated by a thermistor-directed electronic circuit. The thermistor and heating element are lo...

Series 4060 Maintenance Teledyne Analytical Instruments 73 the thyristor gating circuit is continuously delivering gate current from pin 4 of A1, thus maintaining constant full wave AC power to the heater. When the temperature reaches the selected control point, pin 13 voltage is about the same as p...

Series 4060 Appendix Teledyne Analytical Instruments 75 Appendix A.1 Specifications and Initial Settings: Range(s): Refer to Addendum and Testing Results in Appendix B. Power Requirements: Refer to Addendum and Testing Results in Appendix B. Signal Output : Two analog channels: Channel 1: 0-1 VDC an...

Appendix Series 4060 76 Teledyne Analytical Instruments A.2 Recommended Spare Parts List Qty. P/N Description 1 B74671A PC board, Flame guard & anode power supply 1 B79153A PC board, Electrometer 1 C75825A Micro-processor PC board 1 CP2540 Coaxial cable 1 B79154 Sensor Assy. 1 C62371A Display PC...

Series 4060 Appendix Teledyne Analytical Instruments 77 A.3 Drawing List (Refer to the Addendum and Testing Results section of Appendix B for actual drawing list for your application.) D77394 Outline Diagram D77488 Wiring Diagram C76068 Piping Diagram B79159 Schematic, Electrometer PCB B74672 Schema...

Series 4060 Appendix Teledyne Analytical Instruments 79 Appendix B B1 Addendum and Testing Results