Page 3 - ABOUT THIS MANUAL; NOTE; We recommend that this manual and the M200E manual be read in their; REVISION HISTORY; Date
05206H DCN5910 i ABOUT THIS MANUAL This manual is an addendum that supplements the M200E NOx Analyzer manual, p/n 04410; it includes document(s) as listed below. Part No. Name/Description 06185H M201E Spare Parts List (in Section 6.0) Note: Please refer to our Website or Sales for more recent update...
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Page 5 - iii; SAFETY MESSAGES; CAUTION: Hot Surface Warning; CAUTION The analyzer should only be used for the purpose
Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Ammonia Analyzer 05206H DCN5910 iii SAFETY MESSAGES Your safety and the safety of others is very important. We have provided many safety messages throughout this manual; please read these messages carefully. A safety message alerts you to ...
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Page 7 - TABLE OF CONTENTS; PMT; LIST OF FIGURES
05206H DCN5910 v TABLE OF CONTENTS 1.0 M201E AMMONIA ANALYZER .............................................................7 1.1 Theory of Operation...................................................................................................... 10 1.1.1 Minimizing PMT Drift.......................
Page 8 - LIST OF TABLES
vi 05206H DCN5910 Figure 3-6. Analog Output Manual Calibration............................................................................ 33 Figure 3-7. Analog Output Recorder Offset Calibration .............................................................. 34 Figure 4-1. Catalytic Cartridge .........
Page 12 - , with Zero and Span Valve Options Pneumatic Flow; HEORY OF
M201E Ammonia Analyzer Teledyne API Model M201E NH 3 Analyzer Operator Manual 10 05206H DCN5910 Figure 1-3. M201E and M501 NH 3 , with Zero and Span Valve Options Pneumatic Flow 1.1 T HEORY OF O PERATION The Teledyne-API Model M201E analyzer measures ammonia by oxidizing it to nitric oxide by the fo...
Page 13 - TN; Minimizing PMT Drift
Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Ammonia Analyzer 05206H DCN5910 11 and registered as NO x . This location provides the drier with continuous flow, thereby allowing it to stabilize faster. Note: Due to the Nafion® drier, the analyzer has a maximum ammonia range of 2.0 PPM...
Page 14 - Purging the Reaction Cell; PECIAL
M201E Ammonia Analyzer Teledyne API Model M201E NH 3 Analyzer Operator Manual 12 05206H DCN5910 signal. This process improves zero baseline stability by minimizing the effect of PMT sensor drift. 1.1.2 Purging the Reaction Cell As with many chemical reactions the conversion of ammonia in the presenc...
Page 15 - AMPLE
Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Ammonia Analyzer 05206H DCN5910 13 These rules apply also to your calibrator’s internal plumbing. It is highly recommended that you use a M702SS calibrator in conjunction with the M201E. The calibrator has stainless steel plumbing througho...
Page 16 - ppb RMS
M201E Ammonia Analyzer Teledyne API Model M201E NH 3 Analyzer Operator Manual 14 05206H DCN5910 1.4 M201E A NALYZER S PECIFICATIONS Table 1-1. M201E Operating Specifications Ranges 0-50 to 0-2000 ppb in 1 ppb increments (selectable, independent NH 3 , NO, NO 2 , NOx ranges supported) Measurement Uni...
Page 17 - PROCEDURE; DO NOT
05206H DCN5910 15 2.0 CALIBRATION PROCEDURE This section begins with a high-level overview of the calibration procedure for the M201E analyzer. Details are provided starting in Section 2.1: First, take the time to read the M200E manual to familiarize yourself with the Chemiluminescence process. It...
Page 18 - EROING; Important
Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 16 05206H DCN5910 The first time bottled ammonia is connected to the gas dilution system, regulator/calibrator, the TNx reading may take a number of hours to stabilize. 2.1 Z EROING T HE A NALYZER The analyzer can be zeroed...
Page 19 - Table 2-2. Zero Calibration Procedure - Zero Gas Through ZERO Port
Teledyne API Model M201E NH 3 Analyzer Operator Manual Calibration Procedure 05206H DCN5910 17 Table 2-2. Zero Calibration Procedure - Zero Gas Through ZERO Port Step No. Action Comment 1. Press CALZ The M201E enters the calibrate mode from sample mode. The zero gas is supplied through the ZEROinlet...
Page 20 - Table 2-3. NO Calibration Procedure – NO Gas Through the SAMPLE Port
Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 18 05206H DCN5910 operator then manually spans the TN x and NO x channels individually through the user interface. The following Tables outline the manual steps necessary to span the analyzer. Table 2-3. NO Calibration Proc...
Page 21 - Table 2-4. NO Calibration Procedure - NO Gas through the SPAN Port
Teledyne API Model M201E NH 3 Analyzer Operator Manual Calibration Procedure 05206H DCN5910 19 Table 2-4. NO Calibration Procedure - NO Gas through the SPAN Port Step No. Action Comment 1. Press CALS The M201E enters the calibrate mode from sample mode. The NO gas is supplied through the SPAN inlet ...
Page 22 - Samples
Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 20 05206H DCN5910 2.3 S PANNING T HE A NALYZER W ITH A MMONIA G AS The most important criterion an individual can avail themselves of when spanning an analyzer with ammonia gas is “patience”. Ammonia is a very sticky gas an...
Page 23 - Converter; Efficiency
Teledyne API Model M201E NH 3 Analyzer Operator Manual Calibration Procedure 05206H DCN5910 21 Table 2-5. Confirming Ammonia Converter Efficiency Step No. Action Comment 1. Press CAL The M201E enters the calibrate mode from Sample mode. 2. Channel Selection Press TN X then Press ENTR . 3. Range Sele...
Page 24 - Action
Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 22 05206H DCN5910 Table 2-6. NH3 Calibration Procedure – NH3 Gas Through The SAMPLE Port Note: In the example outlined above, the displayed ammonia concentration is being increased by 2.27%. Newer M501 NH 3 , converters s...
Page 25 - Table 2-7. NH3 Calibration Procedure – NH3 Gas through the SPAN Port; ammonia gas is supplied through the
Teledyne API Model M201E NH 3 Analyzer Operator Manual Calibration Procedure 05206H DCN5910 23 Table 2-7. NH3 Calibration Procedure – NH3 Gas through the SPAN Port Step No. Action Comment 1. Press CALS The M201E enters the calibrate mode from Sample mode. The ammonia gas is supplied through the SPAN...
Page 27 - CONFIGURABLE ANALOG OUTPUT OVERVIEW; Table 3-1. Analog Output Data Default Settings; CHANNEL DEFAULT SETTING; ANALOG OUT
05206H DCN5910 25 3.0 CONFIGURABLE ANALOG OUTPUT OVERVIEW There are three different methods to extract concentration data from the E-Series analyzers. By one method, the operator can set up an iDas (internal data acquisition) configuration either through the user display or using TAPI’s windows base...
Page 28 - CNC1 and output A2 to TNxCNC2. Gases with the “1” designation use the
Configurable Analog Output Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 26 05206H DCN5910 Table 3-2. Analog Output Pin-Outs PIN ANALOG OUTPUT VOLTAGE SIGNAL CURRENT SIGNAL 1 V Out I Out + 2 A1 Ground I Out - 3 V Out I Out + 4 A2 Ground I Out - 5 V Out I Out + 6 A3 Ground I Out - 7...
Page 29 - NALOG; this can be done either automatically or manually.
Teledyne API Model M201E NH 3 Analyzer Operator Manual Configurable Analog Output Overview 05206H DCN5910 27 3.1 A NALOG O UTPUT - E LECTRONIC C ONFIGURATION The final step in configuring the analyzer’s four analog output channels is to set the electronic signal type and range of each channel. This ...
Page 31 - manual calibration should only be used for the 0.1V
Teledyne API Model M201E NH 3 Analyzer Operator Manual Configurable Analog Output Overview 05206H DCN5910 29 3.3 S ELECTING A UTO O R M ANUAL A NALOG O UTPUT C ALIBRATION The analog outputs configured for voltage mode can be calibrated either automatically or manually. In its default mode the instru...
Page 32 - Figure 3-3. Auto Or Manual Analog Output Calibration
Configurable Analog Output Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 30 05206H DCN5910 DIAG AIO DATA_OUT_2 AUTO CAL: ON ON ENTR EXIT Exit to Retur n to the m ain Sam ple Di splay DIAG ANALOG I / O C ONFIGU RATION PREV NEXT ENTR EXIT DIAG AIO AOUTS CALIBRATED: NO < SET SET>...
Page 33 - To calibrate the output channels as a group press the following, (; Figure 3-4. Analog Output Group Calibration
Teledyne API Model M201E NH 3 Analyzer Operator Manual Configurable Analog Output Overview 05206H DCN5910 31 To calibrate the output channels as a group press the following, ( Note: this is the recommended calibration approach): DIAG AIO AUTO CALIBRATI NG DATA_ OUT_1 AUTO CALI BRATING DATA_O UT_ 2 …...
Page 34 - Table 3-5. ZERO/SPAN Analog Output Signal Calibration Tolerances; Full Scale; Figure 3-5. Setup For Calibrating Analog Output Signal Levels
Configurable Analog Output Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 32 05206H DCN5910 3.4 M ANUALLY C ALIBRATING A NALOG O UTPUT S IGNAL L EVELS The analog outputs in voltage mode can be manually calibrated to closely match the characteristics of the data recorder. Outputs con...
Page 35 - Figure 3-6. Analog Output Manual Calibration
Teledyne API Model M201E NH 3 Analyzer Operator Manual Configurable Analog Output Overview 05206H DCN5910 33 To make these adjustments the auto calibration feature “DATA_OUT_1 AUTO CAL: OFF” must be turned off for each output channel then press the following: DIAG AIO DATA_OUT_1 C ALIB RATED: YES &l...
Page 36 - Figure 3-7. Analog Output Recorder Offset Calibration
Configurable Analog Output Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 34 05206H DCN5910 3.5 A NALOG O UTPUT R ECORDER O FFSET A DJUSTMENT An offset can be added to individual output channels by pressing the following: DIAG AIO RECORD OFFS ET: 0 MV + 0 0 0 0 E NTR EXI T DI AG ANA...
Page 37 - SCHEDULE; analyzer but with additional maintenance items (; Table 4-1. Preventative Maintenance Schedule; Item; NH; AINTENANCE; The
05206H DCN5910 35 4.0 MAINTENANCE SCHEDULE The maintenance requirements of the M201E are the same as a standard M200E NO x analyzer but with additional maintenance items ( Table 4-1 ). Please refer to Section 13 in the M200E Operator Manual for the M200E maintenance schedule and for maintenance and ...
Page 38 - Converter Rebuild Parts List; EPLACING THE; Turn off power to the converter and allow to cool; . IT IS VERY IMPORTANT; Remove the chassis cover of the M501 NH
Maintenance Schedule Teledyne API Model M201E NH 3 Analyzer Operator Manual 36 05206H DCN5910 Table 4-2. M501 NH 3 Converter Rebuild Parts List Part No. Description KIT000193 RETROFIT, M501NH INNER TUBE w/SCREEN KIT000139 REBUILD, CERAMIC BUSHINGS, M501NH HE0000007 CERAMIC HEATER, 220W@60V M501XX 4....
Page 39 - CAUTION; Ensure power is removed from the
Teledyne API Model M201E NH 3 Analyzer Operator Manual Maintenance Schedule 05206H DCN5910 37 4.3 R EPLACING THE T HERMOCOUPLE The following instructions provide the necessary information to replace the existing thermocouple. Figure 4-2 is provided for reference. You must obtain the following replac...
Page 41 - UTO; , Converter sample flow check
Teledyne API Model M201E NH 3 Analyzer Operator Manual Maintenance Schedule 05206H DCN5910 39 4.4 A UTO Z ERO F LOW C HECK Since the M201E is an ammonia analyzer, the flow through the AutoZero orifice is especially important. Check the AutoZero flow as follows: 1. This procedure should be performed ...
Page 43 - A functional block diagram of the analyzer is shown in; LARM; , converter. If the block temperature warning; AUTION; Be aware that the
05206H DCN5910 41 5.0 ALARMS AND CAUTIONS A functional block diagram of the analyzer is shown in Figure 5-1. 5.1 A LARM During initial warm up the internal Zero/Span factory option may exhibit a “Block Temperature” warning. This can be cleared once the block temperature stabilizes at 50 degrees Cels...
Page 44 - Figure 5-1. M201E Functional Block Diagram
Alarms and Cautions Teledyne API Model M201E NH 3 Analyzer Operator Manual 42 05206H DCN5910 M501NH NH3 CONVERTER CONVERTER MOLYBDENUM DFU FILTER NAFION DRIER GENERATOR OZONE SAMPLE MANIFOLD PHOTONS REACTION CELL MOTHERBOARD I/O I/O OUTPUTS ANALOG DIGITAL ANALOG PREAMP BUS STD AUTOZERO TNx / NOx VAL...
Page 46 - Part Number
M201E Spare Parts List Teledyne API Model M201E NH 3 Analyzer Operator Manual 44 05206H DCN5910 M201E Spare Parts List, Source: PN 06185H (DCN5494) Part Number Description 046030000 AKIT, CH-43, 3 REFILLS 048620200 PCA, SERIAL INTERFACE, w/ MD, E SERIES (USE WITH ACROSSER CPU 041710000) 049310100 PC...
Page 49 - CALCULATING MOLY CONVERTER EFFICIENCIES; URPOSE; API M700 calibrator with O3 Gen option (or equivalent); ARTS; NONE; ROCEDURE
05206H DCN5910 47 7.0 CALCULATING MOLY CONVERTER EFFICIENCIES 7.1 P URPOSE To provide instructions on how to calculate the efficiency of a Moly converter when using a GPT method of testing converters, by using the US EPA method, where the actual concentration of ozone is not a factor in the accuracy...
Page 50 - Note the NO value and input that on line 9 of the data sheet.
Calculating Moly Converter Efficiencies Teledyne API Model M201E NH 3 Analyzer Operator Manual 48 05206H DCN5910 5. Remove the converter bypass and install the converter back into the NOx sample stream, such that the NO sample goes through the converter again and allow the machine to stabilize. Writ...
Page 51 - MOLY TEST DATA SHEET; LOSS
05206H DCN5910 49 MOLY TEST DATA SHEET Line # TEST RESULT 2 LEAK-CHECK (WHEN HOT) YES / NO 3 NO X RESPONSE (MOLY BYPASSED) __________ 4 NO X RESPONSE (MOLY IN-LINE) __________ 5 OUT-GASSING / EATING (NO – NO X ) __________ (>-5 PPB, <5 PPB) 6 (NOx ORIG ) (NO X mode, O 3 off) __________ PPB 7 (...
