Teledyne M5000B - Manuals
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Manual Teledyne M5000B
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i i Model 5000B Teledyne Analytical Instruments Copyright © 1999 Teledyne Analytical Instruments All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed, stored in a retrieval system, or translated into any other language or computerlanguage in whole or in part, in an...
iii Photometric Analyzer Teledyne Analytical Instruments Table of Contents Part I: Control Unit ................................ Part I: 1-1 Part II: Analysis Unit ............................ Part II: 4-1 Appendix ......................................................... A-1
Part I: i Part I: Control Unit Teledyne Analytical Instruments OPERATING INSTRUCTIONS Model 5000B Photometric Analyzer Part I: Control Unit NEMA 4 Bulkhead Mount
Part I: 1-1 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit Introduction 1.1 Overview The Teledyne Analytical Instruments Model 5000B Control Unit, together with a 5000B Analysis Unit, is versatile microprocessor-basedinstrument. Part I, of this manual covers the Model 5000...
Part I: 1-3 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit Hydrogen Fluoride 0–10% Hydroperoxides 0–5% Kerosene 0–500 ppm Ketones 0–1000 ppm Methyl Acetate 0–1000 ppm Methyl Methacrylate 0–1000 ppm Oils 0–1% Olefins 0–500 ppm Pentane 0–300 ppm α -Picolene 0–300 ppm Phenol ...
Part I: 1-5 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit 1.3 Main Features of the Analyzer The Model 5000B Photometric Analyzer is sophisticated yet simple to use. The main features of the analyzer include: • A 2-line alphanumeric display screen, driven by microprocessor...
1-6: Part I Teledyne Analytical Instruments 1 Introduction Model 5000B 1.4 Operator Interface All controls and displays on the standard 5000B are accessible from outside the housing. The instrument has two simple operator controls. Theoperator has constant feedback from the instrument through an alp...
Part I: 1-7 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit -Range This function selects whether analyzer is autoranging or locked on one range. -Standby Places the analyzer in a sleep mode. WARNING: The power cable must be disconnected to fully removepower from the instrum...
1-8: Part I Teledyne Analytical Instruments 1 Introduction Model 5000B Alphanumeric Interface Screen: The backlit VFD screen is an easy- to-use interface between operator and analyzer. It displays values, options,and messages for immediate feedback to the operator. 1.5 Control Section Interface Pane...
Part I: 2-1 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit Installation Installation of Model 5000B Analyzers includes: 1. Unpacking, mounting, and interconnecting the Control/Analysis Section 2. Making gas connections to the system 3. Making electrical connections to the ...
2-2: Part I Teledyne Analytical Instruments 1 Introduction Model 5000B Figure 2-3: Interface Panel of the Model 6600 Control Section For safe connections, ensure that no uninsulated wire extends outside of the terminal blocks . Stripped wire ends must insert completely into terminal blocks. No unins...
Part I: 2-3 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit Figure 2-4: Primary Input Power Connections 115VAC, Fuse Installation: The fuse holders accept 5 x 20 mm, 4.0 A, T type (slow blow) fuses. Fuses are not installed at the factory. Be sure to install the proper fuse ...
2-4: Part I Teledyne Analytical Instruments 1 Introduction Model 5000B 4–20 mA dc Range ID: 8 mA = Range 1, 12 mA = Range 2, 16 mA = Range 3. Figure 2-5: Analog Output Connections Examples: The analog output signal has a voltage which depends on the sample concentration AND the currently activated a...
Part I: 2-5 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit 3 0.3 8.8 4 0.4 10.4 5 0.5 12.0 6 0.6 13.6 7 0.7 15.2 8 0.8 16.8 9 0.9 18.4 10 1.0 20.0 To provide an indication of the range, a second pair of analog output terminals are used. They generate a steady preset voltag...
2-6: Part I Teledyne Analytical Instruments 1 Introduction Model 5000B Normally open Moving contact Normally closedNormally openMoving contact Figure 2-6: Types of Relay Contacts The connectors are: Threshold Alarm 1: • Can be configured as high (actuates whenconcentration is above threshold), or lo...
Part I: 2-7 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit accept 0 V (OFF) or 24 V dc (ON) for remote control of calibration (See Remote Calibration Protocol below .) Zero: Floating input. 5 to 24 V input across the + and – terminalsputs the analyzer into the ZERO mode. E...
Part I: 2-9 Teledyne Analytical Instruments Photometric Analyzer Part I: Control Unit • Which alarms - if any - are tripped (AL-x ON) Each status output is followed by a carriage return and line feed. Three input functions using RS-232 have been implemented to date. They are described in Table 2-4. ...
Photometric Analyzer Operation /Control Unit 3 Part I 3-1 Teledyne Analytical Instruments Operation 3.1 Introduction Although the Model 5000B is usually programmed to your application at the factory, it can be further configured at the operator level, or even, cautiously , reprogrammed. Depending on...
Photometric Analyzer Operation /Control Unit 3 Part I 3-3 Teledyne Analytical Instruments Figure 3-1: Hierarchy of System Functions and Subfunctions System SELF-TEST Self-Test Results Self-Test in Progress Change Yes/No Change Password Verify Password Set track or hold output Set current output CAL-...
3 Operation /Control Unit Model 5000B 3-4 Part I Teledyne Analytical Instruments the appropriate point in the procedure, in a Monospaced type style. Push-buttonnames are printed in Oblique type. 3.3 The System Function The subfuctions of the System function are described below. Specific procedures f...
Photometric Analyzer Operation /Control Unit 3 Part I 3-5 Teledyne Analytical Instruments N o t e : Before setting up an AUTO-CAL, be sure you understand the Zero and Span functions as described in section 4.4, and follow theprecautions given there. Note: If you require highly accurate AUTO-CAL timi...
3 Operation /Control Unit Model 5000B 3-6 Part I Teledyne Analytical Instruments 3.3.2 Password Protection Before a unique password is assigned, the system assigns TAI by default. This password will be displayed automatically. The operator just presses theEnter key to be allowed total access to the ...
Photometric Analyzer Operation /Control Unit 3 Part I 3-7 Teledyne Analytical Instruments arrow keys to change the letters to the proper password. Press Enter to enter the password. In a few seconds, you will be given the opportunity to change this pass- word or keep it and go on. Change Password?&l...
3 Operation /Control Unit Model 5000B 3-8 Part I Teledyne Analytical Instruments When you have finished typing the new password, press Enter . A verifica- tion screen appears. The screen will prompt you to retype your password forverification. Enter PWD To Verify: A A A Use the arrow keys to retype ...
Photometric Analyzer Operation /Control Unit 3 Part I 3-9 Teledyne Analytical Instruments 3.3.4 System Self-Diagnostic Test The Model 5000BF has a built-in self-diagnostic testing routine. Pre- programmed signals are sent through the power supply, output board,preamp board and sensor circuit. The re...
3 Operation /Control Unit Model 5000B 3-10 Part I Teledyne Analytical Instruments 3.3.5 The Model Screen Move the < > arrow key to MORE and press Enter . With MODEL blinking, press Enter . The screen displays the manufacturer, model, and software version information. 3.3.6 Checking Linearity w...
Photometric Analyzer Operation /Control Unit 3 Part I 3-11 Teledyne Analytical Instruments The manual mode only requires entering the values for each correction point into the microprocessor via the front panel buttons. Again, the numberof points required is determined by the user. 3.3.7 Digital Fil...
3 Operation /Control Unit Model 5000B 3-12 Part I Teledyne Analytical Instruments 6 9.0 7 14.0 8 25.0 9 46.0 10 90.0 At a setting of “zero”, the response time is purely set by the electronics to 4.5 seconds. The numbers above can and will change depending on applicationand they merely serve to illus...
3 Operation /Control Unit Model 5000B 3-14 Part I Teledyne Analytical Instruments This function and the TRACK/HOLD feature will prevent false alarms while performing remote or autoscheduled calibrations. These functions arenot applicable if the calibration is initiated through the front panel. To en...
3 Operation /Control Unit Model 5000B 3-16 Part I Teledyne Analytical Instruments 3.3.13 Show Negative The analyzer defaults to not to show negative readings on the analyze mode only. This affects the analog outputs too by pressing the UP or DOWN key, theanalyzer can be set to display negative readi...
Photometric Analyzer Operation /Control Unit 3 Part I 3-17 Teledyne Analytical Instruments zero calibration is to be performed automatically or manually. Use the DÑarrow keys to toggle between AUTO and MAN zero settling. Stop whenAUTO appears, blinking, on the display. Select zeromode: AUTO Press En...
Photometric Analyzer Operation /Control Unit 3 Part I 3-19 Teledyne Analytical Instruments 3.4.2 Span Cal The Span function on the menu is used to span calibrate the analyzer. Span calibration can be performed in either the automatic or manual mode. Make sure the span fluid is flowing to the instrum...
3 Operation /Control Unit Model 5000B 3-20 Part I Teledyne Analytical Instruments Use the DÑ keys to toggle between AUTO and MAN span settling. Stop when MAN appears, blinking, on the display. Press Enter to move to the next screen. Span Val: 2Ø.ØØ %<ENT> To begin span Use the < > arrow ...
3 Operation /Control Unit Model 5000B 3-22 Part I Teledyne Analytical Instruments offset to be entered.4. Do a manual run to check. Reintroduce the zero calibration fluid. Start azero on the analyser but this time enter the offset value.5. At the end of the zero function, check that the instrument r...
3 Operation /Control Unit Model 5000B 3-24 Part I Teledyne Analytical Instruments • Latching? Ltch: Y/N (Yes/No). • To define the setpoint, use the < > arrow keys to move the blinking over to AL1: ####. Then use the DÑ arrow keys to change thenumber. Holding down the key speeds up the incremen...
Photometric Analyzer Operation /Control Unit 3 Part I 3-25 Teledyne Analytical Instruments Select rangemode: MANUAL If above screen displays, use the DÑ arrow keys to Select MANUAL, and press Enter. Select range to run—> Ø1 Ø2 Ø3 CAL<— Use the < > keys to select the range: 01, 02, 03, or...
3 Operation /Control Unit Model 5000B 3-26 Part I Teledyne Analytical Instruments The concentration ranges can be redefined using the Range function Manual screen, and the application fluides can be redefined using the System function, if they are not already defined as necessary. CAUTION: Redefinin...
Photometric Analyzer Operation /Control Unit 3 Part I 3-27 Teledyne Analytical Instruments Figure 3-2 illustrates these schemes graphically. Figure 3-2: Examples of Autoranging Schemes 0 0.01 0.1 80 90 100
3 Operation /Control Unit Model 5000B 3-28 Part I Teledyne Analytical Instruments 3.7 The Analyze Function Normally, all of the functions automatically switch back to the Analyze function when they have completed their assigned operations. Pressing the Escape button in many cases also switches the a...
Photometric Analyzer Operation /Control Unit 3 Part I 3-29 Teledyne Analytical Instruments AUTOCAL FILSOLL HOLD CAL-HOLD-TIMER MORE Select MORE and press ENTER one more time ALGORITHM APPLICATION MORE OUTPUT: 4MA Now you will be able to select the APPLICATION and ALGO- RITHM set-up functions. 3.8.1 ...
3 Operation /Control Unit Model 5000B 3-30 Part I Teledyne Analytical Instruments scale setting until amplifier saturation is reached. Below amplifier saturation, theoverrange readings are accurate UNLESS the application uses linearization overthe selected range. To program the ranges, you must firs...
Photometric Analyzer Operation /Control Unit 3 Part I 3-31 Teledyne Analytical Instruments to the analyzer from the computer. 3.8.2 The Curve Algorithm Screen The Curve Algorithm is a linearization method. It provides from 1 to 9 intermediate points between the ZERO and SPAN values, which can benorm...
3 Operation /Control Unit Model 5000B 3-32 Part I Teledyne Analytical Instruments Repeat the above procedure for each of the data points you are setting (up to nine points: 0-8). Set the points in unit increments. Do not skip numbers. Thelinearizer will automatically adjust for the number of points ...
Part I: Control Unit/Analysis Unit Maintenance 3 Part I: 4-1 Teledyne Analytical Instruments Maintenance Aside from normal cleaning and checking for leaks at the gas connections, routine maintenance is limited to replacing filter elements and fuses, andrecalibration. WARNING: SEE WARNINGS ON THE TIT...
3 Maintenance Model 5000B Photometric Analyzer 4-2: Part I Teledyne Analytical Instruments Figure 4-1: Removing Fuse Block Cap and Fuse from Housing 2. Replace fuse by reversing process in step 1. 4.2 System Self Diagnostic Test NOTE: Always run self diagnostic with the intended zero fluid. 1. Press...
Part I: Control Unit/Analysis Unit Maintenance 3 Part I: 4-3 Teledyne Analytical Instruments Preamp 0 O K >0 means that some of the ten gains of the amplifier have a large offset. The number is acode that tells which of the ten gtains have thelarge offset. Cell (detector) 0 O K >0 means that t...
3 Maintenance Model 5000B Photometric Analyzer 4-4: Part I Teledyne Analytical Instruments WARNING: HAZARDOUS VOLTAGES EXIST ON CERTAIN COMPONENTS INTERNALLY WHICH MAY PERSISTFOR A TIME EVEN AFTER THE POWER IS TURNEDOFF AND DISCONNECTED. The 5000B Control Units contain the following major components...
Part II: i Part II: Analysis Unit Teledyne Analytical Instruments OPERATING INSTRUCTIONS Model 5000B Photometric Analyzer Part II: Analysis Unit NEC or ATEX Type 5000B - GP, Rack, Panel (Integral or Remote) 5000 - GP, Bulkhead (Z-Purged in Div II or Zone 2 areas) I, II, B, C, D (Integral) 5000B-(X-P...
4–1 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 4.0 Operations Before shipment, TAI calibrates the analyzer for your application when feasible. Calibration data is listed in the Appendix. Prior to calibration, TAIchecks the electroni...
4–2 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 4.1 Control Functions 4.1.1 Analysis Section, fully explosion proof, Z or X purged Nema enclosure or Cenelec Purged (pending). The control functions for the analysis section are located...
4–3 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies The control unit digital display must handle functions for both the analysis section and the control module. 4.2 Start-p Information contained in this paragraph is based on the premise ...
4–4 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 4.2.2 Pre-Start-up Electrical Checkout After the preliminary procedures have been accomplished (refer to Prelimi- nary Inspection and Control Settings, above), the integrity of the syst...
4–5 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 3. If the analyzer section has been equipped with the automatic zero SOL option, the zero solenoid device in the accessory samplingsystem should have energized the instant power was est...
4–6 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 4.3 Calibration Standardization Fluids Two standardization fluids are necessary to calibrate the analyzer: 1. Zero Fluid: The zero standard fluid must have a composition similar to the ...
4–8 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies instrument is set up to analyze, then the SPAN control must beadjusted for a full scale reading, i. e., 200 ppm water in EDC. 10. Re-check the ZERO setting with zero fluid. 11. If desir...
4–9 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies A zero may be established with a reproducible simulated (offset) zero absorbance fluid in the sample cell of the analyzer. Whenpossible this fluid should be stable for H2O content and s...
4–10 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies as the off-line method used to verify the process variables. Below is an example of an on-line calibration when measuring0-200ppm water in liquid TDI (assumes TDI is a toxic liquid ats...
4–11 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies optical filters. These optical filters are stable and are chosen to indicate themeasured component at the required instrument wavelengths. Therefore,future, faster, yet much simpler ca...
4–12 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies period). In this case, nitrogen or dry air (typically-100OF dewpoint or 2ppmwater) can be used. Manually switch in the zero offset check from the control unit to operate the zero solen...
4–13 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies always be corrected using the calibration zero and/or span features. SUMMARY The zero and/or span calibration of 5000 series photometric Teledyne analyzers can bequickly verified manua...
4–15 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 5000B Analyzer Cell Nitrogen in - dry purgeoutof cell when manuallyzeroing/spanning SampleFlowmeter.2-2 GPH By-PassFlowmeter2-30 GPH Pressure ReliefValve V-621 Maximum inlet pressure &...
4–17 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 4.4 Operational Theory Cont'd The energy source for the analyzer is most commonly provided by as a high intensity quartz iodine lamp located in the source module. Quartz iodinewas chos...
4–18 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies direct meter indication, which greatly eases the task of balancing the systemduring initial system installation and periods of calibration. The DC voltage levels are fed to a logarithm...
4–19 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies Figure 4-1. Optical System 4.4.2 Sample cell The sample cell, generally constructed of 316SS, is located in the path of the NIR radiation, between the source and the detector modules. ...
4–20 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 2. The entire sample module is separately controlled to maintain the sample temperature during analysis. 3. The sample is temperature compensated for by software while inputing thetemp...
4–21 Operations/Analysis Unit 4 Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 15 VDC Co a rse Zero Co ntrol Se lec tor Switc h MEASREF ZERO Powe r Line Volta g e Re g ula tor Tra nsforme r 5A S1 115 VAC 60 Hz Inp ut F ro m D e te c tor M o du le Prehe a ter Te...
4–22 4 Operations/Analysis Unit Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies 4.4.3 Power See Figure 4-3. The power to the analyzer unit, enables the switching functions, and temperature control for the detector compartment. With the microprocessor control unit,...
Part II: Maintenance/Analysis Unit Maintenance 5 Part II: 5-1 Teledyne Analytical Instruments Maintenance 5.0 Routine Maintenance 5.1 Automatic operation and routine operational duties The system operates continuously without adjustment. Under normal condi- tions, after you program the system for au...
5 Maintenance Model 5000B Photometric Analyzer 5-2: Part II Teledyne Analytical Instruments 3. Verify that the chart recorder contains a normal display. 4. Verify that the recorder has a sufficient supply of chart paper and ink. 5.3 Routine Maintenance Keep the sample lines and components, including...
A-1 Photometric Analyzer, 5000B Appendix Teledyne Analytical Instruments Appendix A-1 Specifications 5000B Digital Control Module: Ranges: Four Programmable Ranges, field selectablewithin limits (application dependent) and AutoRanging Display: 2 line by 20 alphanumeric VFD accompaniedby 5 digit LED ...
A-2 Appendix Models 5000B Teledyne Analytical Instruments Typical Analytical Performance Specifications: ( will vary per application ) Accuracy: ±2% of full scale or better, application dependent Noise: Less than ±1% Diurnal: Less than 1% per 20 o F (10 o C (source/detector dependent) Sample Cell: S...
A-3 Photometric Analyzer, 5000B Appendix Teledyne Analytical Instruments Enclosure Purging: Purge air startup*:40 – 80 PSI (3 – 6 BAR), 0.5 CFM (15 L / min) Purge optical path*:15 – 30 PSI (1 – 2 BAR), 10 cc/min, purity of Nitrogen, - 110 °F (-80 °C) dewpoint * If ordered with purge option Other Fea...
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