Page 2 - Teledyne Analytical Instruments; Copyright © 2004 Teledyne Analytical Instruments
Series 4030 Teledyne Analytical Instruments Copyright © 2004 Teledyne Analytical Instruments All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed, stored in a retrieval system, or translated into any other language or computer language in whole or in part, in any f...
Page 3 - Teledyne Analytical Instruments i; Safety Messages; GENERAL; Technician Symbol; No
Series 4030 Teledyne Analytical Instruments i Safety Messages Your safety and the safety of others are very important. We have provided many important safety messages in this manual. Please read these messages carefully. A safety message alerts you to potential hazards that could hurt you or others....
Page 4 - Teledyne Analytical Instruments ii; Occasionally, some instruments are customized for a particular
Series 4030 Teledyne Analytical Instruments ii CAUTION: THE ANALYZER SHOULD ONLY BE USED FOR THE PURPOSE AND IN THE MANNER DESCRIBED IN THIS MANUAL. IF YOU USE THE ANALYZER IN A MANNER OTHER THAN THAT FOR WHICH IT WAS INTENDED, UNPREDICTABLE BEHAVIOR COULD RESULT POSSIBLY ACCOMPANIED WITH HAZARDOUS ...
Page 5 - Teledyne Analytical Instruments iii; Additional Safety Information; DANGER; COMBUSTIBLE GAS USAGE
Series 4030 Teledyne Analytical Instruments iii Additional Safety Information DANGER COMBUSTIBLE GAS USAGE WARNING This is a general purpose instrument designed for usage in a non-hazardous area. It is the customer's responsibility to ensure safety especially when combustible gases are being analyze...
Page 6 - Teledyne Analytical Instruments iv; Line voltages and line related voltages such as
Series 4030 Teledyne Analytical Instruments iv system. See the procedures for purging and leak checking this instrument on the following pages. If toxic gases or other hazardous materials are introduced into the sample system, the same precautions regarding leak checking and purging apply to the sam...
Page 7 - Teledyne Analytical Instruments v; Switch off the power to the Analyzer and remove the main (line)
Series 4030 Teledyne Analytical Instruments v Procedure for Removal of Internal Inaccessible Shock Hazards CAUTION: SERVICING OR MAINTENANCE OF THE ANALYZER SHOULD ONLY BE DONE BY SUITABLE TRAINED PERSONNEL. TO AVOID THESE INACCESSIBLE HAZARDOUS VOLTAGES WHEN SERVICING THE SERIES 4060, PERFORM EACH ...
Page 8 - Teledyne Analytical Instruments vi
Series 4030 Teledyne Analytical Instruments vi DEPENDING ON THE APPLICATION, MAY ALSO USE TOXIC GASES. IT IS THEREFORE, THE CUSTOMER'S RESPONSIBILITY TO ENSURE THAT PROPER TRAINING AND UNDERSTANDING OF THE PRINCIPLES OF OPERATION OF THIS EQUIPMENT ARE UNDERSTOOD BY THE USER. SINCE THE USE OF THIS IN...
Page 9 - Introduction; Teledyne Analytical Instruments Series 4030 Total Hydrocarbon; Main Features of the Analyzer; The Analyzer is sophisticated yet simple to use. A dual display on
Introduction Teledyne Analytical Instruments 7 Introduction Teledyne Analytical Instruments Series 4030 Total Hydrocarbon (THC) Analyzer is designed to measure the quantity of hydrocarbons present in a heated sample gas, such as gaseous mixtures or ambient air in various industrial applications. The...
Page 10 - Principle of Operation
Introduction Teledyne Analytical Instruments 8 2. High resolution, accurate readings of concentration. 3. Versatile analysis with three user-definable analysis ranges. 4. Microprocessor based electronics: 8-bit CMOS microprocessor with 32 KB RAM and 128 KB ROM. 5. Auto ranging allows analyzer to aut...
Page 11 - Using a built-in pump, the heated Sample from the Sample Selector
Introduction Teledyne Analytical Instruments 9 on the customer’s requirements. The appropriate power cord for your unit has been shipped with this instrument. 1.4 Applications . Monitoring the ambient air for Total Hydrocarbons in chemical and petrochemical plants. . Fugitive emission monitoring. . ...
Page 12 - Sample System
Introduction Teledyne Analytical Instruments 10 The Series 4030 Analyzer is composed of three subsystems: 1. Sample System 2. Detector Cell 3. Electronic Signal Processing, Display and Control 2.2 Sample System The Analyzer contains two (2) separate isothermal chambers controlled by individual PID t...
Page 13 - The Piping diagram is in the rear of this manual. A 10 port-switching
Introduction Teledyne Analytical Instruments 11 2.2.2 Gas Flow Control System The Piping diagram is in the rear of this manual. A 10 port-switching valve is used to control and direct gas flows to the FID detector. The fixed volume sample loop ensures the same volume of sample injection in the Analy...
Page 14 - The thermistor acts as the sensor in the flame guard circuit. Its
Introduction Teledyne Analytical Instruments 12 The anode-igniter, as its name implies, serves two functions. When relay K2 at PCB part number B74671 is energized, the coil becomes an electrical heating element that glows red-hot and ignites the hydrogen fuel. When relay K2 at B74671 is de-energized...
Page 15 - The electrode section of the cell may be removed for inspection by
Introduction Teledyne Analytical Instruments 13 Figure 2-1: Flame Ionization Cell The electrode section of the cell may be removed for inspection by turning off the power, disconnecting the electrode lead plug, and removing the screws, which retain the electrode assembly in the sensor body. 2.3.1 El...
Page 17 - Installation; Unpacking the Analyzer
Installation Teledyne Analytical Instruments 15 Installation Installation of the Series 4030 Analyzer includes: 1. Unpacking 2. Mounting 3. Gas connections 4. Electrical connections 5. Testing the system. 3.1 Unpacking the Analyzer Although the Analyzer is shipped with all the materials you need to ...
Page 18 - User Connections; All user connections are made on the rear panel. Consult the input-
Installation Teledyne Analytical Instruments 16 Regardless of configuration, the analyzer/system must be installed on a level surface with sufficient space allocated on either side for personnel and test equipment access. Subject to the foregoing, the Analyzer/system should be placed as close to the...
Page 19 - Gas connections to the instrument are made at the 1/8”or 1/4”
Installation Teledyne Analytical Instruments 17 Figure 3-1: Gas Connections Gas connections to the instrument are made at the 1/8”or 1/4” stainless steel tube fittings provided on the rear panel. Note that the Purge and Sensor Vent fittings are 1/4” while all other gas connections are 1/8”. If the S...
Page 20 - When connecting the various gas lines to the system, be absolutely; CAUTION; THE GASES USED MUST BE OF THE; Figure 3-1 shows the Series 4030 rear panel. There are connections
Installation Teledyne Analytical Instruments 18 Before tubing is connected to the system, it must be decontaminated to rid it of hydrocarbon deposits. Using a small torch, heat each length of tubing, while passing nitrogen through it, until it glows red. Begin at the nitrogen source end and proceed ...
Page 21 - Figure 3-2: Equipment Interface Connector Pin Arrangement
Installation Teledyne Analytical Instruments 19 THE ANALYZER WITH ITS FASTENING SCREWS. ULTIMATELY, IT IS THE INSTALLER WHO ENSURES THAT THE CONNECTIONS PROVIDE ADEQUATE EMI/RFI SIELDING. 3.3.3.1 P RIMARY I NPUT P OWER The power cord receptacle and fuse block are located in the same assembly. Insert...
Page 22 - fourth set of outputs may be set to any of the following functions:; Pin; Channel 1, negative ground
Installation Teledyne Analytical Instruments 20 Both the first and third set of outputs as well as the second and fourth set of outputs may be set to any of the following functions: - THC -- Total hydrocarbon as measured in the first phase of detection. The output is the percentage of the selected r...
Page 23 - Threshold Alarm 1; Can be configured as high (actuates when concentration is above
Installation Teledyne Analytical Instruments 21 3.3.3.5 A LARM R ELAYS The nine alarm-circuit connector pins connect to the internal alarm relay contacts. Each set of three pins provides one set of Form C relay contacts. Each relay has both normally open and normally closed contact connections. The ...
Page 25 - A serial digital input/output for local network protocol. At this; Description
Installation Teledyne Analytical Instruments 23 3.3.3.7 N ETWORK I/O A serial digital input/output for local network protocol. At this printing, this port is not yet functional. It is to be used in future options to the instrument. Pins 13 (+) and 29 (–). 3.3.3.8 Pin Out Table The following table su...
Page 26 - The input functions using RS-232 that have been implemented
Installation Teledyne Analytical Instruments 24 30 31 32 Exhaust Solenoid Hot 33 Sample Solenoid Hot 34 Range 4 Contact/ not used 35 Range 4 Contact/not used 36 Alarm 3 NC Contact 37 Alarm 3 NO Contact 38 Range 1 Contact 39 Range 2 Contact 40 41 42 Alarm 2 NC Contact 43 Alarm 2 NO Contact 44 Alarm 2...
Page 27 - The RS-232 protocol allows some flexibility in its; Parameter Setting; Normally, four supporting gases of different composition (see
Installation Teledyne Analytical Instruments 25 Implementation: The RS-232 protocol allows some flexibility in its implementation. Table 3-6 lists certain RS-232 values that are required by the Model 4030 implementation. Table 3-6: Required RS-232 Options Parameter Setting Baud 2400 Byte 8 bits Pari...
Page 28 - : THE GASES USED MUST BE OF THE; The sample bypassed by the back-pressure regulation system vents
Installation Teledyne Analytical Instruments 26 CAUTION : THE GASES USED MUST BE OF THE HIGHEST QUALITY, ULTRA ZERO GRADES, AS SHOWN BELOW. FAILURE TO DO SO WILL RESULT IN CONTAMINATION AND FAILURE TO DETECT LOW CONCENTRATIONS OF HYDROCARBONS. AIR: USE ULTRA ZERO GRADE AIR WITH THC LESS THAN 0.1 PPM...
Page 29 - Operation; Placing the System in Operation; Set the air tank regulator to 30 psig.
Operation Teledyne Analytical Instruments 27 Operation 4.1 Placing the System in Operation 1. Plug the power in the AC power inlet in the back of the Analyzer and the Sample Selector Unit. 2. Allow at least 2 hours warm-up (heat up sensor & sample system) after making the air adjustment describe...
Page 30 - Note: Adjust fuel settings only when the red LED (flame failure; Figure 4-1: Front Panel View of Regulator and Gages; Ignition; Observe that after warm up count down timer reaches zero (timer to
Operation Teledyne Analytical Instruments 28 4.2.4 Fuel 1. Open the main valve on the tank and set the fuel tank pressure regulator to 30 psig. 3. Adjust the Fuel regulator until its pressure gauge reads the recommended pressure of 3.5 psig. Note: Adjust fuel settings only when the red LED (flame fa...
Page 31 - Verification of the Flame Guard Circuit; by
Operation Teledyne Analytical Instruments 29 the temperature controller is maintaining the temperature set point) and the red flame failure lamp is on. See Figure 4-1. The Series 4030 will automatically attempt a flame ignition sequence following the warm up period, which has been preset at the fact...
Page 32 - Choose auto ranging or select a fixed range of analysis
Operation Teledyne Analytical Instruments 30 Depending on the specifics of the application, this might include all or a set of the following procedures: 1. Setting system parameters 1. Establish a security password, if desired, requiring operator to log in 2. Establish and start an automatic calibra...
Page 33 - ANALYZE
Operation Teledyne Analytical Instruments 31 4.4.1 Default Parameters The versatility of this analyzer usually results in significant changes being made to parameters over the course of time to better suit a particular application. Occasionally processes change requiring alteration to alarms, ranges...
Page 34 - Analysis Mode; AUTOCAL; Note: All menus time out after 15 (fifteen) seconds elapse with; ANALYSIS SCREEN
Operation Teledyne Analytical Instruments 32 particular key it will be typed as text using all caps. Example: this is the ENTER key. Screen Modes: Times New Roman 12 pt. italic. Example: Analysis Mode or Setup Mode. Screen Readout: Arial Narrow, 12 pt bold. Example: AUTOCAL or Zero in 12 days. 4.4.3...
Page 35 - ESCAPE
Operation Teledyne Analytical Instruments 33 - Dynamic (real time) FID input level - Time spent in mode - Range - Activity indicator LINE 2 display mode 2 data: - Current analysis mode - Analysis TOTAL AREA from most recent pass of current mode. - Time spent in mode - Range - Activity Indicator 3. W...
Page 36 - SPAN; MAIN MENU
Operation Teledyne Analytical Instruments 34 saving the value . The value will revert to the original before modification (if any). 4.4.4 Menu Structure The 4030 screen setup consists of several classes of screens and items. No item occupies more than 1 line. It is important to read and understand t...
Page 37 - MODIFIABLE ITEM
Operation Teledyne Analytical Instruments 35 11. MODIFIABLE ITEM screens have a flashing value somewhere in the line. 4.4.4.1 MAIN M ENUS The MAIN MENU consists of 13 functions you can use to customize and check the operation of the analyzer. They are listed here with brief descriptions: 1. AUTO-CAL...
Page 38 - An exhaustive list of menu messages is provided as follows.
Operation Teledyne Analytical Instruments 36 ENTER it. The analyzer will immediately start that function, unless password restrictions have been assigned. (Password assignment is explained in Section 4.4.10). 4.4.4.2 E XPANDED MENUS An exhaustive list of menu messages is provided as follows. AUTOCAL...
Page 42 - AUTOCAL is not available for standard configurations of the; GAIN TOO HIGH; line of the display, and
Operation Teledyne Analytical Instruments 40 ----------------------- STANDBY Switch to Sleep Mode ENTER-YES ESCAPE-NO notification if logged out ----------------------- Access Restricted Re-enter Password ----------------------- 4.4.5 Setting up an AUTO-CAL AUTOCAL is not available for standard conf...
Page 43 - Setup; Enter
Operation Teledyne Analytical Instruments 41 To setup the GAIN : 1) From the Analysis Screen, press an arrow key to enter the Setup Mode . The VFD will display the first 2 lines of functions available. ________________________________________________ -> GAIN ADJUST PASSWORD ______________________...
Page 44 - Note: If you use password security, it is strongly advised to keep; any key; Enter a Password
Operation Teledyne Analytical Instruments 42 Note however, that the instrument can still be used for analysis without entering the password. To defeat security the password must be entered. Note: If you use password security, it is strongly advised to keep a copy of the password in a separate, safe ...
Page 45 - Enter a new Password
Operation Teledyne Analytical Instruments 43 < Enter > The last <Enter> enters the password. < Escape > Steps back to the previously entered letter or, if on the first letter, returns to the MAIN MENU. If the correct password has been entered the 4040 now allows access to all the S...
Page 46 - Reenter a new Password; Press to advance to the next letter; Note: If you log off the system using the
Operation Teledyne Analytical Instruments 44 ________________________________________________ Reenter a new Password 'A' 'A' 'A' ________________________________________________ Note that the new password has been replaced by 'A' as placeholder characters. This is to ensure that the wrong password i...
Page 47 - Note: The self diagnostics are run automatically by the analyzer
Operation Teledyne Analytical Instruments 45 Pressing <Enter> will logout the current user and protect the system from unauthorized changes to parameters. If user has LOGGED OUT, then only the following SUB MENU procedures may be executed: 17. PASSWORD 18. LOGOUT (which only repeats the logout...
Page 48 - > Start the diagnostic testing routine by pressing; Span
Operation Teledyne Analytical Instruments 46 ________________________________________________ < Enter or Escape > Start the diagnostic testing routine by pressing <Enter> or cancel out by pressing <Escape>. If you pressed <Enter> the self-test routine will begin and after a f...
Page 49 - Pressing enters the SPAN mode in the SMP phase first.
Operation Teledyne Analytical Instruments 47 The first line determines whether a span calculation will be performed for THC. The second line determines whether a span calculation will be preformed for SMP. The third line allows the user to modify the span target value for THC calibration. The fourth...
Page 50 - Note: For the purpose of example, Alarm 2 has been set differently
Operation Teledyne Analytical Instruments 48 AL-1 20.00 ppb AL-1 SOURCE THC AL-2 ACTIVE AL-2 LOW AL-2 FAILSAFE AL-2 LATCHING AL-2 50.00 ppb AL-2 SOURCE SMP ________________________________________________ Note: For the purpose of example, Alarm 2 has been set differently than Alarm 1. Note: An alarm...
Page 51 - RELEASING A LATCHED ALARM: When alarm conditions are
Operation Teledyne Analytical Instruments 49 only during the time the concentration is above the trip point. If that alarm were LATCHING, the alarm condition would persist (even though the concentration is no longer above the trip point), until the user released it. RELEASING A LATCHED ALARM: When a...
Page 52 - The value of the upper limit of the currently selected range (AUTO
Operation Teledyne Analytical Instruments 50 The value of the upper limit of the currently selected range (AUTO or MANUAL) affects the voltage and current of the analog outputs on the rear of the analyzer as well as contact closures indicating which range is current. The Analog outputs on the rear o...
Page 53 - Offset
Operation Teledyne Analytical Instruments 51 4.4.14 Analog output Adjustment The software in this instrument provides a way to enter to manage the analog output of the analyzer FOR ANALOG CHANNEL 1 ONLY . To access the offset function: < ▲▼ > From the MAIN MENU, scroll to the ANALOG ADJUST fun...
Page 54 - If these 2 values are modified and entered and accepted, then the; Advanced User Functions; The Model 4030 provides additional functions for tailoring the
Operation Teledyne Analytical Instruments 52 'Gain: ' plus the Offset value plus a value that is proportionate to the number indicated to the right of 'GAIN:' . If these 2 values are modified and entered and accepted, then the analog output will be affected in like manner in ANALYSIS MODE. That is, ...
Page 55 - Recommended Spare Parts List
Appendix Teledyne Analytical Instruments 53 Recommended Spare Parts List Qty. P/N Description 1 B74671 PC board, Flame guard & anode power supply 1 B74677 PC board, Electrometer-amplifier 1 B30927 PC board, Temperature control 1 C75825A Micro-processor PC board 1 A46128 Coaxial cable 1 B-13207 S...
Page 56 - Analytical Instruments; Drawing List; Model 4030 Outline diagram
Appendix Teledyne Analytical Instruments 54 Send orders to: TELEDYNE INSTRUMENTS Analytical Instruments 16830 Chestnut Street City of Industry, CA 91749-1580 Telephone: (626) 934-1500 Fax: (626) 961-2538 Web: www.teledyne-ai.com or your local representative. Email: [email protected] Drawing List ...