Page 2 - OTICE
The information contained in this document is subject to change without notice. Rosemount Analytical's system of NGA 2000 Modular Gas Analyzers and Controllers are patented, under U.S. Patent5.787.015. Manual Part Number 748410-AAugust 1999Printed in U.S.A. Rosemount Analytical Inc. 4125 East La Pal...
Page 3 - ONTENTS; REFACE; Glossary; ECTION
C ONTENTS 748410-AAugust 1999 i Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 P REFACE Purpose/Safety Summary .................................................................................P1 Glossary .........................................................................
Page 5 - Warranty
C ONTENTS 748410-AAugust 1999 iii Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 S ECTION 4. M AINTENANCE AND T ROUBLESHOOTING 4.1 Overview ....................................................................................................27 4.2 Fuses ........................
Page 6 - IGURES
C ONTENTS 748410-A August 1999 iv Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 F IGURES 1-1 CLD Analyzer Module Flow Diagram .......................................................... 31-2 CLD Analyzer Module - Top View ........................................................
Page 7 - URPOSE; WARNING: AUTHORIZED PERSONNEL
P REFACE 748410-AAugust 1999 P1 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 P URPOSE /S AFETY S UMMARY The purpose of this manual is to provide the procedures for the installation, operation andmaintenance of the Platform and the System Accessories of the NGA 2000 System...
Page 8 - WARNING: TOXIC AND OXIDIZING GAS
P REFACE 748410-A August 1999 P2 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 WARNING: TOXIC AND OXIDIZING GAS This module generates ozone which is toxic by inhalation and is a strong irritantto throat and lungs. Ozone is also a strong oxidizing agent. Its presence isdetec...
Page 9 - WARNING: INTERNAL ULTRAVIOLET LIGHT; the trash, incinerate or flush down the sewer.; WARNING: HAND INJURY HAZARD
P REFACE 748410-AAugust 1999 P3 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 WARNING: INTERNAL ULTRAVIOLET LIGHT Ultraviolet light from the ozone generator can cause permanent eye damage.Do not look directly at the ultraviolet source. Use of ultraviolet filtering glassesi...
Page 10 - WARNING: POSSIBLE EXPLOSION HAZARD
P REFACE 748410-A August 1999 P4 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 WARNING: POSSIBLE EXPLOSION HAZARD Ensure that all gas connections are made as labeled and are leak free.Improper gas connections could result in explosion or death. CAUTION: OVER-VOLTAGE SPIKING...
Page 11 - LOSSARY; The Operator Interface plus the Controller Board.
P REFACE 748410-AAugust 1999 P5 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 G LOSSARY Analyzer Module The module that contains all sensor/detector components for development of a PrimaryVariable signal; includes all signal conditioning and temperature control circuitry. ...
Page 12 - Power Supply
P REFACE 748410-A August 1999 P6 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 Power Supply Any of a variety of components that provides conditioned power to other NGA 2000components, from the Power Supply Board that plugs into the front of the Backplane in astand-alone ins...
Page 13 - C ambient; PECIFICATIONS; See Outline and Mounting Dimensions, Figure 2-4
P REFACE 748410-AAugust 1999 P7 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 S PECIFICATIONS - G ENERAL M EASUREMENT S PECIES : NO, NOx R ANGES : 0 to 10 ppm through 0 to 10,000 ppm NO, NOx R EPEATABILITY : ± 0.5% of fullscale (at constant temperature) M IN . D ETECTABLE ...
Page 14 - Filtered to <2 microns
P REFACE 748410-A August 1999 P8 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 S PECIFICATIONS - S AMPLE T EMPERATURE : 0 ° C to 55 ° C (32 ° F to 131 ° F) T OTAL F LOW RATE : (Externally measured) 900 to 2200 cc/min. withbackpressure regulator pressure adjusted to 344 hPa(...
Page 15 - Current Operator and Service Training Schedule
P REFACE 748410-AAugust 1999 P9 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 C USTOMER S ERVICE , T ECHNICAL A SSISTANCE AND F IELD S ERVICE For order administration, replacement Parts, application assistance, on-site or factory repair,service or maintenance contract info...
Page 16 - NAMUR; OCUMENTATION; 48410 Instruction Manual (this document); OMPLIANCES; FM
P REFACE 748410-A August 1999 P10 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 NAMUR 97-C219 N96 D OCUMENTATION The following Chemiluminescense Detector Analyzer Module instruction materials areavailable. Contact Customer Service or the local representative to order. 74841...
Page 17 - NTRODUCTION; VERVIEW
I NTRODUCTION 748410-AAugust 1999 1 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 1 1.1 O VERVIEW This manual describes the Chemiluminescence (CLD) Analyzer Module of RosemountAnalytical's NGA 2000 Series of gas analysis components (See Figures 1-1 and 1-2). The CLD Analyz...
Page 18 - NO; EATURES
I NTRODUCTION 748410-A August 1999 2 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 1 NO + O 3 → NO2* + O 2 NO 2 * → NO 2 + red light As NO and O3 mix in the reaction chamber, the intensity of the emitted red light ismeasured by a photodiode and is proportional to the concen...
Page 19 - IGURE
I NTRODUCTION 748410-AAugust 1999 3 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 1 TEE 1/8T KYNAR VENT CAPILLARY 70cc/min 4 PSIG PUMP CAPILLARY 1/8 OD TEFLON VALVE C NC NO TEE 1/8TKYNAR TOP CONNECTOR,GLASS BLUE NOx TO NO CONVERTER CONNECTOR,GLASSBLUE CONNECTOR, MALE1/8T-3...
Page 21 - NSTALLATION; NPACKING; CAUTION: HAND INJURY HAZARD; Refer to Section 2-4 for electrical connections.; OCATION; The analyzer should be installed within
I NSTALLATION 748410-AAugust 1999 5 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 2 2.1 U NPACKING If the Chemiluminescence (CLD) Analyzer Module is received as a separate unit, carefullyexamine the shipping carton and contents for signs of damage. Immediately notify thesh...
Page 22 - Operating ambient temperature is 0; ASES; NOTE
I NSTALLATION 748410-A August 1999 6 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 2 F IGURE 2-1. A NALYZER M ODULE I NSTALLATION INTO I NSTRUMENT P LATFORM Unrestricted air flow to the rear of the Analyzer Module is critical to itsperformance and reliability. Operating amb...
Page 24 - in a background of nitrogen is recommended as span gas. For maximum
I NSTALLATION 748410-A August 1999 8 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 2 2.4.3 S PECIFICATIONS Calibration Gases Either U.S.P. breathing grade air or nitrogen is recommended for use as zero gas. A mixtureof NO or NO 2 in a background of nitrogen is recommended a...
Page 25 - Leak Test; LECTRICAL
I NSTALLATION 748410-AAugust 1999 9 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 2 At no time should ozonator gas pressure exceed 2070 hPa-gauge (30 psig).Damage to internal components may occur if this pressure level is exceeded. Leak Test The CLD Analyzer Module is comp...
Page 26 - CLD
I NSTALLATION 748410-A August 1999 10 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 2 F IGURE 2-3. F RONT P ANEL C ONTROLS AND E LECTRICAL C ONNECTIONS Metering Valve Flow Balance Sample Regulator 250 V 24V 1 +2 -3 GND LON 1 LON 2 CLD T 6A Regulator AdjustSlot Network1 Conn...
Page 29 - ISPLAYS; Run; UN
S TARTUP AND O PERATION 748410-AAugust 1999 13 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 3 3.1 OVERVIEW Prior to initial startup, the user should leak test the module as outlined in Section 2. For the remainder of this section, Analyzer Module interconnection with a Pl...
Page 30 - TARTUP
S TARTUP AND O PERATION 748410-A August 1999 14 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 3 DISPLAY MESSAGE DESCRIPTION TYPE BAROMETER System Barometer WARNING BLOCK FET Heater Current WARNING BLOCK THRESH CLD Threshold Temperature WARNING BLOK TEMP Block Temperature WA...
Page 31 - INDING; 3 . 2 p p m N O
S TARTUP AND O PERATION 748410-AAugust 1999 15 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 3 After the warm-up period (about one hour for the CLD Analyzer Module), all modules arecompletely functional. Establish that correct ozonator air pressure and sample flow rate are...
Page 33 - ALIBRATION; Home Escape Map
S TARTUP AND O PERATION 748410-AAugust 1999 17 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 3 F IGURE 3-6. T YPICAL H ELP S CREEN 3.5 C ALIBRATION Under the Expert Controls and Setup menu, use the ↓ arrow key to select Analyzer Module Setup, then select Calibration Gas Li...
Page 34 - Select Zero Offset, press ENTER, adjust the value to 32700 with the; ONVERTER; Two conditions reduce the efficiency of the converter:
S TARTUP AND O PERATION 748410-A August 1999 18 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 3 It is recommended, after initial startup, that the CLD Analyzer Module is calibrated at leastonce every eight hours. This practice should continue until experience indicates that...
Page 36 - A cylinder of nitric oxide standard gas consisting of NO in N
S TARTUP AND O PERATION 748410-A August 1999 20 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 3 3.7 M EASUREMENT OF C ONVERTER E FFICIENCY It is the responsibility of the user to measure efficiency of the NO 2 -to-NO converter during initial startup and thereafter at interv...
Page 38 - Reset converter temperature setpoint 20; UBNORMAL
S TARTUP AND O PERATION 748410-A August 1999 22 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 3 In the initial measurement, after lowering the temperature setpoint in Step 2, theefficiency will normally be less than 92%. 14. Reset converter temperature setpoint 20 ° C highe...
Page 39 - NO C; A. TYPICAL TEST SETUP
S TARTUP AND O PERATION 748410-AAugust 1999 23 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 3 F IGURE 3-7. M EASURING E FFICIENCY OF NO 2 TO NO C ONVERTER NO in AIR ADDED OZONATOR OFF a-b b a c-d c OZONATORON N 2 90 80 85 20 0 A. TYPICAL TEST SETUP B. TYPICAL TEST RESULTS...
Page 40 - EPLACEMENT OF; The presence of NO; adjustment
S TARTUP AND O PERATION 748410-A August 1999 24 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 3 F IGURE 3-8. C ONVERSION E FFICIENCY AS A F UNCTION OF C ONVERTER T EMPERATURE 3.7.4 R EPLACEMENT OF C ONVERTER If the subnormal conversion efficiency is real, and not due to mea...
Page 41 - OUTINE
S TARTUP AND O PERATION 748410-AAugust 1999 25 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 3 3.8 R OUTINE O PERATION The CLD Analyzer Module is designed to continuously analyze the sample stream.Normally, it is never powered off except for servicing or for a prolonged sh...
Page 43 - WARNING: ELECTRICAL SHOCK HAZARD; Disconnect power to the module(s) prior to replacing components.; USES; The main power fuse may require replacement.
M AINTENANCE AND T ROUBLESHOOTING 748410-AAugust 1999 27 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 4 WARNING: ELECTRICAL SHOCK HAZARD Disconnect power to the module(s) prior to replacing components. This equipment should not be adjusted or repaired by anyone except pro...
Page 45 - ANS
M AINTENANCE AND T ROUBLESHOOTING 748410-AAugust 1999 29 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 4 ASSEMBLED SIDE VIEW Converter Tube 655227 Wrap withaluminum foil Glass Cloth Sensor Heater Jacket 655228 Sensor 655282 4.3 F ANS Refer to Figure 4-1. To replace either ...
Page 46 - except
M AINTENANCE AND T ROUBLESHOOTING 748410-A August 1999 30 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 4 4.5 O ZONATOR Refer to Figure 4-1.To replace the ozonator, remove the two large straps and all tie-wraps,and disconnect the one electrical connection. Reassemble in rev...
Page 47 - Reaction Chamber Installation
M AINTENANCE AND T ROUBLESHOOTING 748410-AAugust 1999 31 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 4 Reaction Chamber Installation To reinstall, hold the housing in the inverted position while sliding the Reaction ChamberO-ring and window into position and the tubing i...
Page 51 - CAUTION: PARTS INTEGRITY; REPLACEMENT PARTS
R EPLACEMENT P ARTS 748410-AAugust 1999 35 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 5 CAUTION: PARTS INTEGRITY Tampering with or unauthorized substitution of components may adverselyaffect safety of this product. Use only factory-approved components for repair. 5.1 RE...
Page 52 - Heater Jacket
R EPLACEMENT P ARTS 748410-A August 1999 36 Chemiluminescense Detector Analyzer ModuleRosemount Analytical NGA 2000 5 655250 CONVERTER REPLACEMENT PARTS NL655228 Heater Jacket NL655227 Tube, Aged NL655282 Temperature Sensor 659753, 659754 DETECTOR REPLACEMENT PARTS NL655235 Heater/Thermostat Assembl...
Page 53 - CLD I; DENTIFICATION; CHEMILUMINESCENCE NO/NOx ANALYZER - CLD
CLD I DENTIFICATION M ATRIX 748410-AAugust 1999 A1 Chemiluminescense Detector Analyzer Module Rosemount Analytical NGA 2000 A Each analyzer is configured per the customer sales order. Below is the CLD sales matrixwhich lists the various configurations available. To identify the configuration of an a...
Page 57 - Rosemount Analytical; ARRANTY
Goods and part(s) (excluding consumables) manufactured by Seller are warranted to be free fromdefects in workmanship and material under normal use and service for a period of twelve (12)months from the date of shipment by Seller. Consumables, glass electrodes, membranes, liquidjunctions, electrolyte...
Page 59 - Field service and repair facilities are located worldwide.; National Response Center; IELD
Field service and repair facilities are located worldwide. U.S.A. To obtain field service on-site or assistance with a service problem, contact (24 hours, 7days a week): National Response Center 1-800-654-7768 I NTERNATIONAL Contact your local Rosemount Sales and Service office for service support. ...
Page 61 - SAMPLE INLET FLOW RATE RESTRICTION; FOR NGA 2000 CLD ANALYZER MODULE; CAUTION; NOTICE; EXTERNALLY RESTRICT SAMPLE FLOW TO LESS THAN 2200 CC/MIN.; PN
I NSTRUCTIONS 015-748335-B Rosemount Analytical SAMPLE INLET FLOW RATE RESTRICTION FOR NGA 2000 CLD ANALYZER MODULE Rosemount Analytical Inc. 4125 East La Palma Avenue • Anaheim, California 92807-1802 • (714) 986-7600 • FAX (714) 577-8006 June 1997 015-748335-B Printed in U.S.A. CAUTION NOTICE EXTER...
Page 63 - ADDENDUM; NSTRUCTION; Read this information and note the conflicts.; ENU
I NSTRUCTIONS 015-748430-A Rosemount Analytical ADDENDUM CLD I NSTRUCTION M ANUAL 748410 Rosemount Analytical Inc. 4125 E AST L A P ALMA A VENUE • A NAHEIM , C ALIFORNIA 92807-1802 • (714) 986-7600 • FAX: (714) 577-8006 A UGUST 1999 • 015-748430-A • P RINTED IN USA This addendum serves as an amendme...
Page 106 - OTES
ADDENDUM 44 of 44 Rosemount Analytical August 1999 748430-A N OTES