Page 5 - Chapter 1
Contents Chapter 1 Introduction ...................................................................................................................1 1.1 Description of manual ..................................................................................................................1 1.2 Syste...
Page 6 - Chapter 4
3.3.3 Electrical and signal ground .........................................................................................34 3.3.4 Electrical conduit .........................................................................................................35 3.3.5 Sample system requirements ..........
Page 7 - Appendices and reference; Appendix A
4.4.18 Recommended spare parts ....................................................................................... 127 4.4.19 Upgrading the embedded software ...........................................................................127 Appendices and reference Appendix A Local operator interfac...
Page 9 - Description of manual; System description; Analyzer assembly; Electronics assembly
1 Introduction This section describes the contents and purpose of the 700XA Gas Chromatograph System Reference Manual , a description of the Model 700XA system, an explanation of the theory of operation, and a glossary of chromatograph terminology. Use this section to get acquainted with the basic e...
Page 10 - Functional description
The GC-to-PC interface provides the user with the greatest capability, ease-of-use, andflexibility. MON2020 can be used to edit applications, monitor operations, calibratestreams, and display analysis chromatograms and reports, which can then be stored asfiles on the PC’s hard drive or printed from ...
Page 11 - Gas chromatography process model; Software description; Embedded GC firmware
In most cases it is essential to use MON2020 to configure and troubleshoot the GC. The PCmay be remotely connected via ethernet, telephone, radio or satellite communications.Once installed and configured, the GC can operate independently for long periods of time. Gas chromatography process model Fig...
Page 13 - Theory of operation; Thermal conductivity detector; Analyzer assembly with TCD bridge
After the equipment/software has been installed and the operation stabilized, automaticoperation can be initiated via an ethernet network. 1.5 Theory of operation The following sections discuss the theory of operation for the GC, the engineeringprinciples and the concepts used. Note See Section 1.7 ...
Page 14 - Detector output during component elution
In the quiescent condition, prior to injecting a sample, both legs of the bridge are exposedto pure carrier gas. In this condition, the bridge is balanced and the bridge output iselectrically nulled. The analysis begins when the sample valve injects a fixed volume of sample into thecolumn. The conti...
Page 15 - Flame ionization detector; Analyzer assembly with FID detector bridge; Liquid sample injection valve
1.5.2 Flame ionization detector The other detector available for the 700XA is the flame ionization detector (FID). The FIDrequires a polarization voltage and its output is connected to the input to a highimpedance amplifier that is called an electrometer. The burner uses a mixture of hydrogenand air...
Page 16 - LSIV cross section; Methanator
LSIV cross section Figure 1-5: The LSIV penetrates the wall of the lower compartment and is held in place by a retainingring. The mounting arrangement is designed to ensure integrity of the flameproofenclosure. The outermost end houses an air-operated piston. Air at 60 PSI is directed by a solenoidv...
Page 17 - Data acquisition; Peak detection
1.5.5 Data acquisition Every second, exactly 50 equally spaced data samples are taken (i.e., one data sampleevery 20 milliseconds) for analysis by the controller assembly. As a part of the data acquisition process, groups of incoming data samples are averagedtogether before the result is stored for ...
Page 18 - Basic analysis computations; Concentration analysis - response factor
Onset is defined where the detector output exceeds the baseline constant, but peaktermination is defined where the detector output is less than the same constant. Sequences of fused peaks are also automatically handled. This is done by testing eachtermination point to see if the region immediately f...
Page 19 - Concentration calculation - mole percentage (without
The response factor calculation, using the external standard, is: AR F n = Arean Caln or HR F n = H tn Caln where ARF n area response factor for component “n” in area per mole percent Area n area associated with component “n” in calibration gas Cal n amount of component “n” in mole percent in calibr...
Page 20 - Concentration calculation in mole percentage (with; Glossary; Auto Zero
CON C n = Arean AR F n or CON C n = H tn HR F n where ARF n Area response factor for component “n” in area per mole percent. Area n Area associated with component “n” in unknown sample. CONC n Concentration of component “n” in mole percent. Ht n Peak height associated with component “n” mole percent...
Page 22 - TCD
RxD, RD, or S in Receive data, or signal in. TCD Thermal conductivity detector. A detector that uses the thermalconductivity of the different gas components to produce anunbalanced signal across the bridge of the preamplifier. The higherthe temperature, the lower the resistance on the detectors. TxD...
Page 23 - Equipment description; 00XA gas chromatograph; Front panel assembly
2 Equipment description and specifications Use the following sections to reference the 700XA equipment description orspecifications. 2.1 Equipment description The 700XA consists of a copper-free aluminum explosion-proof chamber, and a front panelassembly. The chamber is divided into two compartments...
Page 24 - The switch panel; Valve switch from switch panel set to “OFF”; AUTO
The switch panel The switch panel contains a network of on/off switches that allow you to manually controlthe GC’s stream and analytical valves. 8-stream switch panel (left) and 18-stream switch panel (right) Figure 2-2: There are two types of switch panels: 8-stream and 18-stream. The 8- stream swi...
Page 26 - CPU; Valves; The local operator interface
Status LEDs (Bottom of switch panel) Figure 2-6: • CPU - Green light blinks continuously while the GC is running. • Valves - Turns green if the valves are functioning automatically; turns red if the valves’ automatic settings have been overridden. Note During GC start up, all LEDs turn on for approx...
Page 27 - Upper compartment; Lower compartment
• 8 infrared-activated touch screen keys that eliminate the requirement for amagnetic pen. • Complete GC status, control and diagnostics, including full chromatogram display. See Appendix A for more information about operating the LOI. 2.1.2 Upper compartment The upper compartment contains the follo...
Page 28 - Optional AC/DC power supply; Mechanical pressure regulators; The mechanical pressure regulators
- Heater/Solenoid board The card cage also has four additional slots for the following optional PCBs: - A second preamp board - A second heater/solenoid board - Two optional communications boards WARNING! The explosion-proof housing should not be opened when the unit is exposed to anexplosive enviro...
Page 29 - Equipment specifications; Utilities
The mechanical pressure regulators and gauges are used to set and monitor the pressureof the carrier gas flow through the GC's columns, as well as the pressure of the FID air andfuel (H 2 ). The regulators and gauges are located beneath the GC. 2.2 Equipment specifications 2.2.1 Utilities Use the fo...
Page 30 - Electronic hardware
Type Specification Mounting • Floor mount • Pole mount: - 2” (60.3 mm) - 3” (89.0 mm) - 4” (114.3 mm) • Direct wall mount Power • 24V DC standard (21-30 V DC operating voltage range); MAX 150 watts • (optional) 100-120/240 V AC; 50-60 Hz Note Voltage range includes line voltage variations. Instrumen...
Page 35 - Precautions and warnings
3 Installation and setup This section provides instructions for installing and commissioning the 700XA. Installing a 700XA involves the following steps:1. Observing precautions and warnings. 2. Planning site location and mounting arrangement. 3. Obtaining supplies and tools. 4. Mounting the unit. 5....
Page 37 - Installation considerations; XA mounting arrangements
Note When the vapor regulators and flow switches are fitted they must be suitably certified with theratings Ex d IIC Gb T5/T6/T4 and for a minimum ambient temperature range Ta = -20°C to +60°C . Note Where right angle bend cable adaptors are used they shall be appropriately certified and shallinterf...
Page 38 - Wall mount
3.2.1 Wall mount The simplest mounting arrangement is the wall mount. If ‘Wall Mount’ is specified on thesales order, the unit will be shipped with a wall mount installation kit. Four locations on themounting ears are available for support. 1. The unit is most easily mounted if a pair of 7/16-inch d...
Page 39 - Pole mount
2. Maneuver the GC so that the notches in the mounting ears can be placed over thebolts on the wall and then place the washers over the bolts. 3. Install the second pair of bolts with washers and then tighten all the bolts. 3.2.2 Pole mount The pole mount arrangement uses an additional plate and spa...
Page 40 - Floor mount
7. Place the nuts with washers on the upper bolts and then tighten all bolts. WARNING! Until all bolts are tight, the unit should be supported to prevent unforeseen accidents. 8. Adjust the lower bracket to align the bolts with the plate. Tighten the bolts. 3.2.3 Floor mount If ‘Floor Mount’ is spec...
Page 41 - Gas chromatograph wiring; Power source wiring; Signal wiring
3.3 Gas chromatograph wiring 3.3.1 Power source wiring Follow these precautions when installing power source wiring: • All wiring, as well as circuit breaker or power disconnect switch locations, mustconform to the CEC or NEC; all local, state, or other jurisdictions; and companystandards and practi...
Page 42 - Electrical and signal ground
• All process signal wiring should be of a single, continuous length between fielddevices and the GC. If, however, the length of the conduit runs require that multiplewiring pulls be made, the individual conductors must be interconnected withsuitable terminal blocks. • Use suitable lubrication for w...
Page 43 - Interior ground lug, lower enclosure; Electrical conduit
Interior ground lug, lower enclosure Figure 3-4: • Resistance between the copper-clad steel ground rod and the earth ground mustnot exceed 25 Ohms. • On ATEX-certified units, the external ground lug must be connected to thecustomer’s protective ground system via 9 AWG (6mm 2 ) ground wire. After the...
Page 44 - Sample system requirements
• All conduit fitting-threads, including factory-cut threads, must be coated with ametal-bearing conducting grease prior to assembly. • Temporarily cap the ends of all conduit runs immediately after installation toprevent accumulation of water, dirt, or other contaminants. If necessary, swab outcond...
Page 45 - Preparation; Site selection
Dryers and Filters Use small sizes to minimize time lag and prevent back diffusion. • Install a minimum of one filter to remove solid particles. Most applica-tions require fine-element filters upstream of the GC. The GC includes a2-micron filter. • Do use ceramic or porous metallic type filters. Do ...
Page 46 - If any parts or assemblies appear to have been damaged in shipment; Required tools and components
Note The serial number for MON2020 is located on the back of its CD-ROM case. 2. If your GC is configured with an FID, remove the vent plug from the FID outlet. The vent plug has a tag attached to it that reads “REMOVE VENT PLUGS PRIOR TOOPERATION”. Failure to remove the cap could result in a perfor...
Page 47 - Supporting tools and components; Installation; DC power supply
• 14 AWG (American Wire Gauge), 18 MWG (Metric Wire Gauge) or larger electricalwiring and conduit to provide 120 or 240 volts AC, single phase, 50 to 60 Hertz,from an appropriate circuit breaker and power disconnect switch. See guidelines in Section 3.3 . • Digital volt-ohm meter with probe-type lea...
Page 48 - 4 VDC power connection on the back plane
CAUTION! Check the unit prior to wiring to determine if it is equipped for DC power. Failure to observethis precaution may damage equipment. To connect a 24 VDC power source to the GC, do the following: 1. Locate the plug-together termination block inside the electronics enclosure. 24 VDC power conn...
Page 49 - Optional AC/DC power converter
Location of entries for wiring on the under side of the lower enclosure Figure 3-6: Use the following table for the DC power wiring details: Attribute Wire Color + (positive) red – (negative) black Note Do not disconnect the factory-installed ground wire. 3. The backplane board that connects to the ...
Page 50 - AC/DC termination block; Connect the sample and other gas lines
1. Locate the plug-together termination block inside the electronics enclosure, atopthe power supply and adjacent to the card cage. AC/DC termination block Figure 3-7: WARNING! Do not connect the AC power leads without first ensuring that AC power source isswitched OFF. Failure to follow this warnin...
Page 53 - RS-485 serial port terminals; RI; CD; Installing the analog modem
3.5.4 Maximum effective distance by communication protocol type The table below lists the maximum distance at which the indicated protocol can transmitdata without losing effectiveness. If longer runs are required, the use of a repeater or othertype of extender will be necessary to maintain the prot...
Page 54 - Connecting to the GC via the analog modem
1. Start MON2020 and connect to the GC. 2. Select I/O Cards... from the Tools menu. The I/O Cards window displays. 3. Change the Card Type for the appropriate I/O slot to Communication Module - Modem . 4. Click Save . MON2020 displays the following message: The GC must be rebooted for the ROC Card c...
Page 55 - Connecting directly to a PC using the GC’s Ethernet port
6. Make sure that the Comm Address matches the Modbus Id from the Communication window. 7. Select the appropriate modem from the Modem drop-down list. The Edit Telephone Number dialog box displays. 8. Enter the modem’s telephone number and click OK . The Modem Properties window displays. 9. Click OK...
Page 56 - Ethernet ports on the backplane
Ethernet ports on the backplane Figure 3-10: 1. Plug one end of the Ethernet cable into the PC’s Ethernet port and the other end intothe GC’s RJ45 socket on J22 on the backplane. 2. Locate the set of switches at SW1, directly beneath the Ethernet port on the backplane. Flip the switch that is labell...
Page 57 - SW1 switches on the back plane; Start; Properties
SW1 switches on the back plane Figure 3-11: Note Make sure the SW1 switch is set to off (1) before connecting the GC to your local network;else, the GC will disrupt the local network's functioning. 3. Wait for 20 seconds and then do the following to ensure that the server hasprovided an IP address t...
Page 58 - Using MON2020 to connect to the GC; Troubleshooting DHCP connectivity issues
7. To configure the PC to accept IP addresses issued from the GC, select the Obtain an IP address automatically and Obtain DNS server address automatically check boxes. 8. Click OK to save the changes and to close the Internet Protocol (TCP/IP) Properties window. 9. Click OK to close the Local Area ...
Page 59 - CPU board link lights; Connecting directly to a PC using the GC’s serial port
CPU board link lights Figure 3-12: 4. Do the following to ensure that your network adapter is enabled: a. Go to Start → Control Panel → Network Connections . b. Check the status of the Local Area Connection icon. If the status appears as Disabled , right-click on the icon and select Enable from the ...
Page 61 - Connecting directly to a PC using the GC’s wired; Crimped CAT 5 cable
c. Select the New GC text and type in a new name for the GC connection. Note You can enter optional but helpful information about the connection in the Short Desccolumn. d. Select the new GC’s Direct check box. e. Click the Direct button located at the bottom of the GC Directory window. The Direct C...
Page 62 - Wired Ethernet terminal block on the backplane; Field wiring to TB11
Note The GC can be connected (or remain connected) to the local network on TB11 on the back planewhile the DHCP feature is being used. Wired Ethernet terminal block on the backplane Figure 3-15: Use the following schematics as a guide to wiring the GC via its Phoenix connector at TB11. Figure 3-16 s...
Page 63 - Assigning a static IP address to the GC
CAT5e wiring to TB11 Figure 3-17: Once you have wired the cable to the Ethernet terminal, plug the other end into a PC or awall jack. See Section 3.5.12 to continue configuring the GC. 3.5.12 Assigning a static IP address to the GC To configure the GC with a static IP address, do the following: 1. S...
Page 64 - Add; File
5. Log off the GC. 6. Access the backplane, which is located in the GC’s lower enclosure. Port locations on the backplane Figure 3-18: 7. If you are setting up a static IP address for the Ethernet port at J22, and you alsointend to connect to your company’s local area network, do the following: a. L...
Page 65 - Discrete digital I/O wiring; Discrete digital inputs; TB7 on the backplane
10. Select the new profile and click Ethernet... Enter the GC’s static IP address in the IP address field. 11. Click OK . The Ethernet Connection Properties for New GC window closes. 12. Click Save on the GC Directory window. 13. Click OK to close the GC Directory window. 14. Select Connect... from ...
Page 66 - Discrete Digital Inputs
Note The discrete digital input terminals are optically isolated from the GC's other circuitry. 2. Route digital I/O lines appropriately, especially in the case of the explosion-proofenclosure. There are connections for five digital inputs and five digital output lines, as indicatedin the following ...
Page 67 - Typical field wiring of a ROC800 DI module; Typical wiring
Typical field wiring of a ROC800 DI module Typical wiring Figure 3-20: Terminal Label Definition 1 1 CH 1 Positive 2 2 CH 2 Positive 3 3 CH 3 Positive 4 4 CH 4 Positive 5 5 CH 5 Positive 6 6 CH 6 Positive 7 7 CH 7 Positive 8 8 CH 8 Positive 9 COM Common 10 COM Common To connect the ROC800 DI module ...
Page 68 - Discrete digital outputs; TB3 on the backplane
Note Twisted-pair cables are recommended for I/O signal wiring. The module’s terminal blocksaccept wire sizes between 12 and 22 AWG. A minimum of bare wire should be exposed toprevent short circuits. Allow some slack when making connections to prevent strain. 2. Insert the exposed end into the clamp...
Page 69 - Discrete Digital Outputs; Optional discrete digital inputs; Optional card slots
Discrete Digital Outputs (continued) Table 3-2: TB3 Function Pin 10 DIG_OUT NC4 Pin 11 DIG_OUT ARM4 Pin 12 DIG_OUT NO4 Pin 13 DIG_OUT NC5 Pin 14 DIG_OUT ARM5 Pin 15 DIG_OUT NO5 Note Form-C relays are single-pole double-throw (SPDT) relays that have three positions: normally closed( NC ); an intermed...
Page 70 - Typical field wiring of a ROC800 DO module
Typical field wiring of a ROC800 DO module Typical wiring Figure 3-23: Terminal Label Definition 1 1+ Positive discrete output 2 COM Discrete output return 3 2+ Positive discrete output 4 COM Discrete output return 5 3+ Positive discrete output 6 COM Discrete output return 7 4+ Positive discrete out...
Page 71 - Analog input wiring; Analog inputs on the blackplane; TB10 on the black plane; Factory settings for analog input switches
2. Insert the exposed end into the clamp beneath the termination screw. 3. Tighten the screw. 3.5.14 Analog input wiring All 700XAs have at least two analog inputs. An additional four analog inputs are availablewith a ROC800 AI-16 card that can be installed into one of the optional slots in the card...
Page 72 - Selecting the input type for an analog input; Typical wiring for line-powered transmitters
Factory settings for analog input switches Figure 3-25: Note To set an analog input to accept a voltage (0-10 VDC) source, flip the appropriate switch in theopposite direction from that shown in Figure 3-25 . Selecting the input type for an analog input An analog input can be set to either voltage (...
Page 73 - Optional analog inputs
Typical wiring for line-powered transmitters Figure 3-26: Optional analog inputs When plugged into one of the optional card slots on the card cage, the ROC800 AI-16 cardprovides four additional analog inputs. The AI channels are scalable, but are typically usedto measure either a 4-20 mA analog sign...
Page 74 - Typical field wiring of a ROC800 AI-16 module
Typical field wiring of a ROC800 AI-16 module Typical wiring Figure 3-28: To connect the ROC800 AI-16 module to a device, do the following: CAUTION! Failure to exercise proper electrostatic discharge precautions—such as wearing a groundedwrist strap—may reset the processor or damage electronic compo...
Page 75 - Analog output wiring; Analog outputs on the backplane
Calibrating a ROC800 AI-16 module To calibrate the ROC800 AI-16 module you must have a PC with the ROCLINK 800Configuration program installed and open. 1. Select the Configure → I/O → RTD Points → Calibration tab. 2. Select an Analog Input . 3. Click Update to request one value update from the input...
Page 76 - Factory settings for analog output switches
TB4 on the black plane Figure 3-29: Analog Outputs Table 3-4: TB4 Function Pin 1 + Loop1 Pin 2 Loop_RTN1 Pin 3 + Loop 2 Pin 4 Loop_RTN2 Pin 5 + Loop 3 Pin 6 Loop_RTN3 Pin 7 + Loop 4 Pin 8 Loop_RTN4 Pin 9 + Loop 5 Pin 10 Loop_RTN5 Pin 11 + Loop 6 Pin 12 Loop_RTN6 Factory settings for analog output sw...
Page 78 - Wiring for customer-powered analog outputs
Wiring and switch settings for customer-powered analog outputs It is possible to furnish power to each analog output while maintaining isolation betweenchannels. Consult the following diagrams before wiring a customer-powered device: 1. This drawing shows the wiring that is necessary to provide powe...
Page 79 - Settings for analog output switches; Optional analog outputs
Settings for analog output switches Figure 3-33: Optional analog outputs When plugged into one of the optional card slots on the card cage, the ROC800 AO cardprovides four additional analog outputs. Each channel provides a 4 to 20 mA current signalfor controlling analog current loop devices. For mor...
Page 80 - Leak checking and purging for first calibration; Checking the GC for leaks
Terminal Label Definition 6 COM Analog output return 7 4+ Positive analog output 8 COM Analog output return 9 N/A Not used 10 N/a Not used To connect the ROC800 AO module to a field device, do the following: 1. Expose the end of the wire to a maximum length of ¼ inch (6.3mm). Note Twisted-pair cable...
Page 81 - Purging carrier gas lines; The Heaters window
7. Repeat Step 5 again. If leaks persist, check the valve ports with a commercial gas leak detector. Do not use a liquid leak detector such as Snoop ® on the valves or components in the oven. 3.6.2 Purging carrier gas lines Purging carrier and calibration gas lines requires power and a PC connected ...
Page 82 - Purging calibration gas lines; System startup
8. Select Control → Auto Sequence . For more information about this function, refer to the MON2020 Software for Gas Chromatographs manual. Note A purging period of 4 to 8 hours (or overnight) is recommended, during which no changesshould be made to the settings described in Step 1 through Step 7 . 3...
Page 83 - Warning and precautions
4 Operation and maintenance 4.1 Warning and precautions WARNING! Observe all precautionary signs posted on the 700XA. Failure to do so can result in injury ordeath to personnel or cause damage to the equipment. CAUTION! Turn off GC before removing a card from the card cage assembly. Failure to do so...
Page 84 - Pt Exp; Resp Factor; Troubleshooting and repair concept; Maintenance checklist
The GC is ready to analyze the sample or validation stream using the 2 Pt Exp and the Resp Factor that were calculated during the LCG and HCG runs. 4.3 Troubleshooting and repair concept The most efficient method for maintaining and repairing the 700XA is a component-replacement concept that allows ...
Page 86 - Routine maintenance procedures; Service programs; Precautions for handling PC assemblies; General troubleshooting
4.4.2 Routine maintenance procedures • To give yourself a basis for comparison in the future, complete the maintenancechecklist at least two times each month. Place the sales order number, date, andtime on the form and file it. • Save a chromatogram of the operating GC on the PC with MON2020. Printc...
Page 94 - Test points; Lower enclosure showing test points on the back plane; Voltage LEDs
Test points Lower enclosure showing test points on the back plane Figure 4-1: The backplane has a set of test points that allow you to measure the voltage output of theBase I/O card. Each test point is labeled with a voltage value that, when measured with avoltmeter, should give a measurement equal ...
Page 95 - Temperature; Heaters...
Voltage LEDs Figure 4-2: The following LEDs are associated with the following GC components: LED GC Component FUSE OPEN Glows red when the fuse has blown or been removed; otherwise, it is not lit. 24 LOOP (Power) Glows green when the current loop for the analog outputs is functioning prop- erly; oth...
Page 96 - FID configuration; Detectors
When viewing the Heater window, the typical heater configuration is as follows: • Heater 1 is the analytical block heater. • Heater 2 is the “high hat” heater. The Temperature column on the Heaters window displays the current temperature; the Current PWM column displays the percentage of power being...
Page 97 - The Detectors window
The Detectors window Figure 4-3: Configure the following fields from the Detectors dialog: • FID Ignition - manual or automatic • Ignition Attempts • Wait Time Between Tries • Igniter ON duration • Flame ON Sense Temperature • Flame OUT Sense Temperature • Electrometer Voltage Note If the FID does n...
Page 98 - Required tools for valve maintenance
Plugged lines, columns, and valves If the lines, columns, or valves are plugged, check the gas flow at valve ports. For areference, use the flow diagram in the drawing package, and remember these pointsabout flow diagrams: • Port-to-port flow paths are indicated by solid or dashed lines. • A dashed ...
Page 99 - XA valves; Valve overhaul
XA valves Figure 4-4: Valve overhaul Note Replacement factory-built XA valves are available. Call your Emerson Process Managementrepresentative for more information. Use the following procedure to overhaul a valve: 1. If you are overhauling a 6-port valve, refer to drawing #CE-22015; If you areoverh...
Page 100 - The torque bolt; Removing and replacing solenoids
The torque bolt Figure 4-5: 8. Holding the lower piston plate, pull the valve straight off the block. The alignmentpins may stick slightly. 9. Remove and discard the old valve diaphragms and gaskets. 10. Clean the sealing surface as required using a non-lint-forming cloth and isopropylalcohol. Blow ...
Page 101 - Detector maintenance; Required tools for TCD maintenance
1. Remove the thermal cover from the upper enclosure. 2. Loosen the ultem thumb screw and tilt the oven on its side to gain access to thesolenoids that are located on the underside of the ultem. 3. Loosen the screws holding the solenoid in place and remove the solenoid. 4. To replace the solenoid, r...
Page 102 - TCD with block; Replacing a TCD
TCD with block Figure 4-6: Replacing a TCD Use the following procedure to remove a TCD assembly from the GC for repair orreplacement: WARNING! Disconnect all electrical power to the unit and ensure the area is free of explosive gases. Failureto follow this warning may result in injury or death to pe...
Page 103 - Components of a TCD block; Removing the FID
Components of a TCD block Figure 4-7: 4. To replace the TCD, reverse the steps taken to remove it. Note The block screws should be tightened with a torque wrench to 20 inch-ounce. 4.4.8 Removing the FID The FID has no replaceable parts. Damage such as a broken RTD or igniter coil will requirethat th...
Page 104 - The FID
The FID Figure 4-8: Use the following procedure to remove an FID from the GC: 1. Disconnect all power to the unit. Allow at least 10 minutes for the components to cool-down. 2. Locate the FID switch, which is on the half-moon-shaped wire terminal board, andflip it to the "off" position. Oper...
Page 105 - The location of the FID switch; LSIV maintenance; Installing a MAT LSIV
The location of the FID switch Figure 4-9: 3. Remove the explosion proof dome and the thermal hood. 4. Remove the screw connecting the termination board to the FID cap. 5. Remove the two screws from the mounting bracket. 6. Unscrew and remove the vent connector. Note Use a backing wrench on the bolt...
Page 106 - MAT LSIV components
MAT LSIV components Figure 4-10: Note For a detailed view of the MAT LSIV’s components, see Figure 4-14 . To install the MAT LSIV, do the following: 1. Install new MAT valve by doing the following: a. Attach the retaining ring from step 6c above to the MAT LSIV.b. Slide the MAT LSIV into the mountin...
Page 107 - Required tools; The LSIV tools
Required tools Although for the most part it is possible to remove or disassemble the LSIV with traditionaltools such as a wrench or pliers, the following tools should have been delivered with yourLSIV-mounted gas chromatograph: • Two 10-mm wrenches (A) • Union coupling wrench (B) • Two 3-mm Allen w...
Page 108 - Removing the MAT LSIV
CAUTION! This unit operates at high temperature. Allow a cool-down period of at least 10 minutes aftershut-down and handle the unit carefully. Failure to follow this precaution may result in injuryor death to personnel. MAT LSIV components Figure 4-12: Note For a detailed view of the MAT LSIV’s comp...
Page 109 - Replacing LSIV seals
700XA after LSIV (A) has been removed Figure 4-13: Replacing LSIV seals Due to the possible damage caused by the presence of solids in the sample stream,combined with the regular, repeated motion of the injection valve stem, LSIV seals mayrequire annual replacement. Note Specific application conditi...
Page 111 - Methanator maintenance
LSIV - exploded view Figure 4-14: 4.4.10 Methanator maintenance The optional methanator, which is a catalytic converter, converts otherwise undetectableCO 2 and/or CO into methane by adding hydrogen and heat to the sample. The methanator requires little maintenance. Operation and maintenance 4 Opera...
Page 112 - Methanator assembly
Note Be sure to insulate the methanator assembly to prevent heat loss. Methanator assembly Figure 4-15: The RTD is replaceable. When replacing it, take care to anchor the RTD cable to the tubingto prevent loosening over time. To replace the RTD, consult drawing #CE-22210, which is available at the b...
Page 113 - Measure vent flow; Measure flow vents; Electrical components
4.4.11 Measure vent flow You will need an accurate flow meter for this measurement. To measure the measure vent flow, do the following: Measure flow vents Figure 4-16: 1. Consult the documentation the Parameter List that was provided with the GC tolearn the appropriate flow rate. 2. Attach a flow me...
Page 114 - Remove the front panel; Remove the switch panel or LOI
To access the card cage, do the following: 1. Ensure electrical power is disconnected from the unit and the environment is safe. 2. Unscrew and remove the front panel. Remove the front panel Figure 4-17: 3. Unscrew and remove the switch panel or LOI. Remove the switch panel or LOI Figure 4-18: The P...
Page 115 - PCBs in the card cage; Replacing AC/DC power supply
PCBs in the card cage Figure 4-19: 4. Note the location and direction of any board removed. Release the catch(es) andremove/replace the circuit board(s) as necessary. Replacing AC/DC power supply The AC/DC power supply is mounted on the left wall of the lower enclosure adjacent to thecard cage and i...
Page 116 - AC/DC power supply located in lower compartment
AC/DC power supply located in lower compartment Figure 4-20: A Cross point #2 Phillips screw driver is required to remove and replace the AC/DC powersupply. To remove and replace an AC/DC power supply, do the following: 1. Remove power to the GC. 2. Unscrew and remove the front panel. Remove the fro...
Page 117 - The card cage
Remove the switch panel or LOI Figure 4-22: 4. If present, remove the clear cover from the card cage. The card cage Figure 4-23: 5. Unplug all the cards in the card cage but do not remove them. 6. Unscrew the three switch panel connector posts. Remove the washers as well. 7. Lift the card cage with ...
Page 118 - Factory settings for jumpers and switches; Preamp board factory jumper setting
12. Remove the nut just above the power supply. The power supply may now be twistedfree of the attaching stud and lifted from its cradle. Remove the power supplycarefully to avoid damage due to wire interferences. 13. Maneuver the new power supply into the cradle, ensuring that the wires are free to...
Page 119 - Communications
Heater/Solenoid board factory jumper setting Figure 4-25: Base I/O board factory jumper and switch settings Figure 4-26: Backplane factory switch setting Figure 4-27: 4.4.14 Communications The 700XA has four serial communications ports: Port 0, Port 1, Port 2, and Port 3, which isa dedicated PC-to-G...
Page 120 - Maximum distance by communication type; Changing the line drivers
Name Location Connector Type ETHERNET1 J22 RJ45 (DHCP-enabled) ETHERNET2 TB11 4-wire terminal block Ethernet ports on the backplane Figure 4-28: Maximum distance by communication type Communication Type Maximum Length RS-232 50 feet RS-422/RS-485 4000 feet Ethernet (CAT5) 300 feet Changing the line ...
Page 121 - Applications; OK
Port Name Port Mode Terminal Block Locationon the back plane Communication Modes Sup-ported Port 0 RS232 TB1 Modbus ASCII/RTU RS422,RS485 TB2 Port 1 RS232 TB5 Modbus ASCII/RTU RS422,RS485 TB6 Port 2 RS232 TB8 Modbus ASCII/RTU RS422,RS485 TB9 Port 3 (DB9 connec-tor) RS232 J23 (LAPTOP-PC) Modbus ASCII...
Page 123 - Serial port switches on the Base I/O board
Serial port switches on the Base I/O board Figure 4-32: 10. Make sure that SW12 is set to the down position or Port 0 will not function. Note Ordinarily SW12 should never be adjusted. It is used by the factory for testing purposes. If itwas somehow set to the top, be sure to return it to its factory...
Page 125 - Terminal block locations on the backplane; Optional RS-232 serial ports; Tools; Communications module - RS232
Terminal block locations on the backplane Figure 4-33: 15. Once the appropriate termination blocks are wired correctly, you can start up theGC. Optional RS-232 serial ports It is possible to install an optional RS-232 board in one or both of the expansion I/O slotsprovided on the GC’s card cage in t...
Page 126 - Use PPP protocol for serial connection (use SLIP if unchecked); Configuring the optional RS-485 serial port to function as an
5. Turn off the GC. 6. Install the RS-232 board into the appropriate I/O card slot in the GC’s card cage. 7. Start the GC. Optional RS-485/RS-422 serial ports It is possible to install an optional RS-485 board in one or both of the expansion I/O slotsprovided on the GC’s card cage in the electronics...
Page 127 - Installing or replacing a FOUNDATION fieldbus module; The FOUNDATION fieldbus module
Termination IN Termination OUT J4 In Out J6 In Out TB1 Wire Terminals RS-485 (Half Duplex/2-Wire) RS-422 (Full Duplex/4-Wire) A RxTx+ Rx+ B RxTx- Rx- Y NC Tx+ Z NC Tx- 4.4.15 Installing or replacing a FOUNDATION fieldbus module The FOUNDATION fieldbus module Figure 4-34: The FOUNDATION fieldbus modu...
Page 128 - Removing a FOUNDATION fieldbus module; Installing a FOUNDATION fieldbus module
Removing a FOUNDATION fieldbus module Note Be sure to properly ground yourself before performing this procedure. To remove the module, do the following: 1. Unscrew the two LOI post tips. The FOUNDATION fieldbus module can now bedetached from the card cage. 2. Remove the two screws that attach the FO...
Page 129 - FOUNDATION fieldbus wiring on the backplane; Connecting the GC’s FOUNDATION fieldbus module to a; Carrier board showing connector at TB1
FOUNDATION fieldbus wiring on the backplane Figure 4-35: Connecting the GC’s FOUNDATION fieldbus module to a Fieldbus segment The FOUNDATION fieldbus module has a terminal at TB1 on the carrier board, which is themiddle card in the stack. This terminal can be used to connect to a fieldbus segment. C...
Page 130 - Connecting the optional ground wire; Carrier board showing ground lug at TB2; Foundation Fieldbus jumper settings
Connecting the optional ground wire If you wish to provide the Foundation Fieldbus module with surge protection, there is aground lug at TB2 on the module’s carrier board, which is the middle card in the stack. Oneend of the ground wire should be attached to this lug nut, and the other end should be...
Page 131 - Preamplifier board; Heater/solenoid driver board; not
Board Jumper Set? LOI J1 Yes For more details, consult the following drawings: Preamplifier board Figure 4-38: JP1 on the preamplifier board should not be set. The preamplifier board is located in slot 1 of the card cage. Heater/solenoid driver board Figure 4-39: JP1 on the heater/solenoid driver bo...
Page 132 - should
The Base I/O board, which is located in slot 3 of the card cage, has three jumpers thataffect the performance of the Foundation Fieldbus. JP1 on the Base I/O board Figure 4-40: JP1 on the Base I/O board should be set. JP2 on the Base I/O board Figure 4-41: JP2 on the Base I/O board should not be set...
Page 133 - JP3 on the Base I/O board; CPU board; OFF
JP3 on the Base I/O board Figure 4-42: JP3 on the Base I/O board has three pins, and the jumper should be set on pins 2 and 3. CPU board Figure 4-43: S3 and S4 on the CPU board should be switched to OFF , which is the left-most position while holding the board right-side up. Operation and maintenanc...
Page 134 - Analog inputs and outputs; Analog output adjustment; Discrete digital inputs and outputs
LOI board Figure 4-44: The J1 jumper is located on the back of the LOI, at the top while holding the LOI right-sideup. It should be set. 4.4.16 Analog inputs and outputs The analog outputs can be calibrated or adjusted with MON2020. However, these outputsshould be measured with a calibrated digital ...
Page 135 - Recommended spare parts; Upgrading the embedded software
4.4.18 Recommended spare parts See Appendix C for the lists of recommended spare parts. The quantities listed in the tables represent the number of spares to cover most contingencies for up to five GCs or for morethan 5 GCs or critical installations. Emerson Process Management, however, offers servi...
Page 137 - The LOI; Light emitting diode indicators
Appendix ALocal operator interface A.1 Interface components for displaying and entering data The local operator interface (LOI) has multiple components that you can use to interactwith the unit. The LOI Figure A-1: A.1.1 Light emitting diode indicators There are three light emitting diode (LED) stat...
Page 138 - LCD screen; The command keys; The arrow keys
The GC is currently running an analysis. The GC has at least one unacknowledged alarm. The GC has an out-of-tolerance or alarm condition that requires an operator action. A.1.2 LCD screen The LCD screen measures 111.4mm by 83.5 mm and is capable of 640 by 4800 VGA pixelresolution, supporting both te...
Page 139 - Pressing a key; Using the local operator interface; Start up
Pressing a key A key is “pressed” by placing a finger on the glass over the associated key hole and thenremoving the finger. Holding a finger over the key hole will cause that key to repeat untilthe finger is removed. A.2 Using the local operator interface A.2.1 Start up Upon starting the GC, the LO...
Page 140 - Navigating menus; Navigating the screen; Cancel
Pressing F1 when “MOVE” is displayed in the green box below it takes the focus inside thescreen so that you can navigate through the controls of the screen using the LEFT, RIGHT,UP and DOWN keys. Pressing EXIT returns the focus to the top level—that is, outside of thescreen. Pressing LEFT or RIGHT a...
Page 142 - Editing numeric fields
When you press a key, a green square will flash in the upper left corner if the key is valid; ifthe key is not valid, a red box will flash in the upper left corder. A.2.4 Editing numeric fields When the focus is on an editable field, pressing F1 (EDIT) will display the Edit Dialogcontaining the fiel...
Page 143 - Editing non-numeric fields; Editing alphanumeric fields; Selecting a check box; Clicking buttons; Selecting radio buttons
The EXIT key cancels any changes that were entered and closes the Edit Dialog, restoringthe previous value to the field. A.2.5 Editing non-numeric fields The function of the keys when editing non-numeric data is context-dependant. Editing alphanumeric fields Alphanumeric fields take numbers (0 - 9) ...
Page 144 - Selecting an item from a list box; Selecting a list box; Selecting an item from a combo box
Selecting an item from a list box 1. Press F1 (SELECT) while focused on the list box to switch it to edit mode. Selecting a list box Figure A-3: 2. Use the UP and DOWN arrows keys to move between the values within the list box. 3. Press ENTER to accept the current selection or press EXIT to abort th...
Page 145 - Selecting a combo box; Entering a date and time
Selecting a combo box Figure A-4: 2. Use the UP and DOWN arrow keys to move between the selections. 3. Press ENTER to select the desired value or press EXIT to restore the combo box’sinitial value. Entering a date and time 1. Press F1 (SELECT) while focused on the Date and Time field and the Enter t...
Page 146 - Setting the time
Entering a date and time Figure A-5: 2. Use the UP and DOWN arrow keys to change the value of the unit—that is, to gofrom January to February, or from 1 to 2. 3. Use the LEFT and RIGHT arrow keys to change units—that is, to go from months toyears or hours to minutes. Note If the focus is on the left...
Page 147 - Screen navigation and interaction tutorial; Navigate to the Application menu
A.3 Screen navigation and interaction tutorial This tutorial, which guides you through the procedure for editing data on a screen, willincorporate all of the preceding information to demonstrate the typical method ofnavigating and interacting with the LOI. You will learn how to perform the following...
Page 148 - The System screen
Note Notice that the green prompt boxes are empty. This means that the F1 and F2 keys areinactive from the Main Menu . 2. Click ENTER. The System screen displays. The System screen Figure A-7: Note Notice the navigation icon in the upper right corner, which indicates that no arrow keys areactive. 3....
Page 149 - You must log in to the GC before editing a screen
You must log in to the GC before editing a screen Figure A-8: Note Notice that there is also a navigation icon on the Login dialog. 7. Click F1 (SELECT) and navigate up or down the list to highlight your user name. Note For the remainder of this tutorial, when referring to the F1 key, the key’s curr...
Page 151 - The Is Multi User Write Enabled? check box
Note If a validation error is found after pressing ENTER, an “Invalid Entry” message displays. PressENTER to close the message and then re-enter your data. 14. Use the down arrow to move to the Is Multi User Write Enabled? check box. The Is Multi User Write Enabled? check box Figure A-11: 15. Press ...
Page 152 - The Is Multi User Write Enabled? check box, no longer checked; The GC Mode field
The Is Multi User Write Enabled? check box, no longer checked Figure A-12: 16. Click F1 (SELECT) again to re-select the check box. 17. Navigate to the GC Mode field. The GC Mode field Figure A-13: 18. Press F1 (SELECT). The Select an Item combo box displays.
Page 153 - The Select an Item combo box; The LOI screens
The Select an Item combo box Figure A-14: 19. Use the DOWN arrow to scroll down to the last item in the combo box. Press ENTER. 20. Press ENTER a second time to save all the changes that were made to the table. Note If you neglect to press ENTER at this point, all of your changes will be lost. 21. P...
Page 155 - The Chromatogram menu
Submenu Command Subcommands Reference Logs/Reports Maintenance Log Figure A-46 Event Log Figure A-47 Alarm Log Figure A-48 Unack Alarms Figure A-49 Active Alarms Figure A-50 Report Display Figure A-51 Control Auto Sequence Figure A-53 Single Stream Figure A-54 Halt Figure A-55 Calibration Figure A-5...
Page 157 - The Live Chromatogram View (Status Mode) screen; The Live Chromatogram View (Advanced Mode) screen
The Live Chromatogram View (Status Mode) screen Figure A-17: Note The blue box displays the current analysis time. The Live Chromatogram View (Advanced Mode) screen Figure A-18:
Page 158 - The Archived Chromatogram (Advanced Mode) screen
Note The blue box displays the current analysis time. The Archived Chromatogram (Advanced Mode) screen Figure A-19: The Live & Archived Chromatogram Viewer Options screen Figure A-20:
Page 159 - The CGM Scaling screen
Note The blue box displays the cursor’s x- (analysis time) and y- (amplitude) coordinates. The CGM Scaling screen Figure A-21: The Chromatogram CDT Table screen Figure A-22:
Page 160 - The Hardware menu
The Chromatogram TEV Table screen Figure A-23: The Chromatogram Raw Data Table screen Figure A-24: A.4.2 The Hardware menu The Hardware menu enables you to view and manage the GC’s hardware components.
Page 162 - The Valves screen; The EPC screen
The Valves screen Figure A-27: Note The usage (Sample/BF1, Dual Column), mode (Auto, Off), and state (green = on, black = off, red =error) of each valve is displayed. See the “Configuring the valves” section of the MON2020 Software for Gas Chromatographs User Manual for more information. The EPC scr...
Page 165 - The Application menu
The Analog Outputs screen Figure A-33: The Installed Hardware screen Figure A-34: A.4.3 The Application menu The Application menu allows you to view the CDT, TEV and streams tables for the GC. The System , Status , and Ethernet Ports screens are also accessible from this menu.
Page 170 - The Logs/Reports menu
The Status screen Figure A-43: The Ethernet Ports screen Figure A-44: A.4.4 The Logs/Reports menu The Logs/Reports menu enables you to view the various reports that are available from the GC.
Page 174 - The Report Display screen; The Control menu
The Report Display screen Figure A-51: A.4.5 The Control menu The Control menu enables you to stop, calibrate, or place on automatic control a sample stream from the analyzer. Refer to the “Control menu” section of the MON2020 Software for Gas Chromatographs User Manual for detailed information rega...
Page 178 - The Stop Now screen; The Manage menu
The Stop Now screen Figure A-58: A.4.6 The Manage menu The Manage menu enables you to change the LOI’s settings, change a user’s password, and log off of the GC to which you are connected. Refer to the “Manage menu” section of the MON2020 Software for Gas Chromatographs User Manual for detailed info...
Page 180 - Troubleshooting a blank LOI screen
The Create PIN screen Figure A-61: The Diagnostic screen Figure A-62: A.5 Troubleshooting a blank LOI screen If the LOI is powered up but the LCD screen is blank, do the following: 1. Unscrew and remove the LOI from the GC.
Page 181 - Jumpers at J105 on LOI motherboard
2. Flip the LOI over to expose its motherboard and associated electronics. Jumpers at J105 on LOI motherboard Figure A-63: 3. Check the jumpers located at J105 on the motherboard. These jumpers control the screen’s power. Tofunction properly, jumper pins 3 and 4 must be set; if they are not, set the...
Page 183 - Carrier gas; Manifold for two carrier gas bottles to GC system
Appendix BCarrier gas installation and maintenance B.1 Carrier gas This appendix provides a description of the optional carrier manifold (P/N 3-5000-050)that permits the connection of two carrier gas bottles, or cylinders, to a gaschromatograph (GC) system. The benefits of this manifold are as follo...
Page 184 - Installation and line purging
V-1 Carrier cylinder 1 Bleed valve V-2 Carrier cylinder 1 Block valve V-3 Carrier cylinder 2 Block valve V-4 Carrier cylinder 2 Bleed valve B.2 Installation and line purging To install and purge the dual-bottle carrier gas manifold, proceed as follows: 1. Install manifold as shown in Figure B-1 . Cl...
Page 185 - Replacing carrier cylinder; Calibration gas
B.3 Replacing carrier cylinder To replace one carrier cylinder without interrupting GC operation, proceed as follows: 1. Turn cylinder valve off. 2. Back off on cylinder pressure regulator until handle turns freely. 3. Remove cylinder. 4. Attach new cylinder to regulator and repeat Steps 3 through 7...
Page 188 - Recommended spare parts for 700XA FID/TCD
0 1 per car-rier CARRIER DRYER ASSEMBLY 2-3-0500-180 Note If a GC has a stream internal switching assembly, then one spare is recommended. Note Application dependent. Please contact your Rosemount Analytical, Inc. representative and providethe GC's sales order number for recommended part number and ...
Page 189 - Recommended spare parts for 700XA FID
0 1 PCA SOLENOID/HEATER DRIVER 2-3-0710-002 0 1 PCA BASE I/O 2-3-0710-003 0 1 PCA BACKPLANE 2-3-0710-005 0 1 PCA MAIN CPU 2-3-0710-007 0 1 PCA FID ELECTROMETER 2-3-0710-014 0 Note 3 ASSEMBLY, POWER SUPPLY (AC) 2-3-0710-053 0 1 ASSEMBLY, MICROFID, XA 2-3-0710-077 0 Note 4 KIT, FIELD, METHANATOR REPLA...
Page 191 - recommendations
Appendix DShipping and long-term storage recommendations The following recommendations should be followed: • For shipping purposes the gas chromatograph should be secured to a woodenpallet, maintained in a vertical position and enclosed in a wood framework with acardboard skin. • Auxiliary equipment...
Page 193 - List of engineering drawings
Appendix EEngineering drawings E.1 List of engineering drawings This addendum contains the following engineering drawings: • BE-22175 Label Set Field Wiring Card 1 (Sheets 1, 2, and 3) • DE-22050 Outline and Dimensional Pole, Wall and Floor Mounting Units, 700XA • CE-22260 Assembly, 6 Port XA Valve,...